| 无溶剂下微波合成吡啶酰胺化合物 |
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| 引用本文： | 罗世霞,朱淮武,张笑一,ZHANG,Xiaoyi.无溶剂下微波合成吡啶酰胺化合物[J].贵州师范大学学报(自然科学版),2009,27(3):116-118. |
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| 作者姓名： | 罗世霞 朱淮武 张笑一 ZHANG Xiaoyi |
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| 作者单位： | 贵州师范大学化学与材料科学学院,贵州,贵阳,550001 |
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| 基金项目： | 教育部“春晖计划”合作科研项目(Z2007-1-52001);;贵州省国际科技合作计划(黔科合外G字[2009]700126) |
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| 摘 要： | 通过微波合成法,在无溶剂条件下,制备了吡啶酰胺化合物2,6-双{N(1′-羟基甲基-2′-羟基-2-(′4″-硝基苯基)乙基]氨甲酰基}吡啶,合成过程无需溶剂,反应速度快,操作简便、安全,过程节能、环保。目标化合物的结构经元素分析、核磁共振氢谱、核磁共振碳谱、红外光谱、紫外光谱进行了表征。
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| 关 键 词： | 微波合成 吡啶酰胺 表征 |
Microwave irradiation synthesis of pyridine-diamides in free solvent |
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| LUO,Shixia,ZHU Huai-wu,ZHANG,Xiaoyi.Microwave irradiation synthesis of pyridine-diamides in free solvent[J].Journal of Guizhou Normal University(Natural Sciences),2009,27(3):116-118. |
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| Authors: | LUO Shixia ZHU Huai-wu ZHANG Xiaoyi |
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| Institution: | School of Chemistry and Materials;Guizhou Normal University;Guiyang;Guizhou 550001;China |
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| Abstract: | 2,6-Bis{N(1′-hydroxymethyl-2′-hydroxy-2′-(4″-nitrophenyl)ethyl]carbamyl}pyridine was synthesized under microwave irradiation in free solvent.The methods had a characteristic of free solvent,fast reaction,simple operation,safety,low energy consumption and environmental protection.The product was characterized by elemental analysis,1H-NMR,13C-NMR,IR and UV spectra. |
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| Keywords: | microwave irradiation synthesis pyridine-amide characterize |
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