| 绞股蓝皂甙的提纯及性质研究 |
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| 引用本文： | 刘晓颖,宋德贵.绞股蓝皂甙的提纯及性质研究[J].安徽大学学报(自然科学版),1996,20(4):56-61. |
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| 作者姓名： | 刘晓颖 宋德贵 |
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| 作者单位： | [1]安徽大学生物系 [2]合肥生化制药厂 |
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| 摘 要： | 采用甲醇、水和乙醇等三种试剂提纯绞股蓝皂甙；其粗品经氧化镁吸附得绞股蓝皂甙精制品。用人参皂甙作标准品，测定３种试剂提取的绞股蓝皂甙的纯度，并用硅胶薄层层析法和红外光谱法测定其化学组成，通过测定结果比较，发现以乙醇为绞股蓝皂甙的提纯试剂的方法最好
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| 关 键 词： | 绞股蓝皂甙，总皂甙量，提纯，达玛烷型结构 |
Research on the purification of Gyp and its properties |
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| Liu,Xiaoying,Zheng,Shilian,Deng,Chuanjun,Sun,Li.Research on the purification of Gyp and its properties[J].Journal of Anhui University(Natural Sciences),1996,20(4):56-61. |
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| Authors: | Liu Xiaoying Zheng Shilian Deng Chuanjun Sun Li |
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| Institution: | Liu Xiaoying Zheng Shilian Deng Chuanjun Sun Li (Department of Biology. Anhui University Hefei 230039) Song Degui (Hefei Biochemical Pharmaceutical Factory 230031) |
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| Abstract: | The experiment, discribed in the artical to the three reagents, namely, methanol, water and ethanol, to purify gyp, and extracts refined Gyp from its remained part which is absorbed by MgO. The purity of Gyp extracted by the three reagents can be measured with Gin Rb1 as a stardard substance, and its chemical structure can be determined through silica gel thin layer chromatography and infra red absorption spectrum. From the comparision among the determenation results, the fact is shown that the application of ethanol is the best method in the purification of Gyp. |
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| Keywords: | Gyp general Gyp quantity purfication dammarane |
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