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| 间溴苯乙酮的合成研究 | |
| 引用本文： | 苏娇莲,林原斌. 间溴苯乙酮的合成研究[J]. 湘潭大学自然科学学报, 2002, 24(4): 54-56 |
| 作者姓名： | 苏娇莲 林原斌 |
| 作者单位： | 1. 湖南工程学院化学化工系,湖南,湘潭,410001 2. 湘潭大学化学学院,湖南,湘潭,411105 |
| 摘 要： | KBrO3是一种优良的纯化芳环溴化剂，在硫酸的催化下温和地转化成HOBr。采用KBrO3作为溴化剂，以溴化苯乙酮为原料合成间溴苯乙酮，并采用正交实验对技术参数进行了优化，得到了温和的反应条件。间溴苯乙酮的收率高达80.5%。 |
| 关 键 词： | KBrO3 间溴苯乙酮 合成 正交实验法 溴化剂 Sandmeyer反应 正交实验 |
| 文章编号： | 1000-5900(2002)04-0054-03 |
| 修稿时间： | 2002-07-30 |
Study on the Synthesis of m-Bromoacetophenone |
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| SU Jiaolian ,LIN Yuanbin. Study on the Synthesis of m-Bromoacetophenone[J]. Natural Science Journal of Xiangtan University, 2002, 24(4): 54-56 | |
| Authors: | SU Jiaolian LIN Yuanbin |
| Affiliation: | SU Jiaolian 1,LIN Yuanbin 2 |
| Abstract: | Potassium bromate, as an excellent brominating agent, was mildly transformed into HOBr by sulfuric acid and was used as brominating agent to produce m -bromoacetophenone for brominating acetophenone. The optimum and mild reaction conditions for the synthesis of m -bromoacetophonone have been determined by orthogonal experiment method. A high yield for m -bromoacetophenone was obtained to be 80.5%. |
| Keywords: | potassium bromate m -bromoacetophenone synthesis orthogonal experiment method |
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