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冰片氧基丙酮的合成及分析
引用本文:张翘楚,钟平.冰片氧基丙酮的合成及分析[J].江西师范大学学报(自然科学版),1993,17(2):157-159.
作者姓名:张翘楚  钟平
作者单位:宜春师专,宜春师专
摘    要:莰烯在硫酸催化下与1.2-丙二醇反应,制得1-冰片氧基-2-丙醇,产率42.6%.1-冰片氧基-2-丙醇用三氧化铬的硫酸溶液氧化后得到冰片氧基丙酮,产率77.6.上述合成的化合物均进行了MS.IR.HNMR分析和评香鉴定.

关 键 词:莰烯  合成香料  冰片氧基丙酮

Synthesis and Analysis of Bornyloxy Propanone
Zhang Xiaochu zhong Ping.Synthesis and Analysis of Bornyloxy Propanone[J].Journal of Jiangxi Normal University (Natural Sciences Edition),1993,17(2):157-159.
Authors:Zhang Xiaochu zhong Ping
Institution:Yichun Teacher' s College
Abstract:The reaction of camphene with 1,3-propanediol in the presence the yield is 42. 6%. The oxidation of 1-bornyloxy 2-propanol by chromic acid affords bornyloxy propanone and the yield is 74. 6%. The products are identified by MS, IR, ' HNMR and their aroma are also determined.
Keywords:camphene  synthesis of perfumes  O-alkylation  oxidation
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