| 固体超强酸TiO_2/SO_4~(2-)催化合成异戊氧基乙酸烯丙酯 |
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| 引用本文： | 游毅,王文峰,唐威.固体超强酸TiO_2/SO_4~(2-)催化合成异戊氧基乙酸烯丙酯[J].福州大学学报(自然科学版),1999(5):88-90. |
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| 作者姓名： | 游毅 王文峰 唐威 |
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| 作者单位： | 福州大学化学系!福建福州350002(游毅，王文峰)，福建医科大学化学教研室!福建福州350004(唐威) |
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| 摘 要： | 在固体超强酸ＴｉＯ２／ＳＯ２ －４ 催化下， 由异戊氧基乙酸和烯丙醇合成异戊氧基乙酸烯丙酯－ 考察了催化剂用量、原料配比、反应时间等因素对产物产率的影响， 确定了最佳反应条件， 产物产率８８－４ ％ ， 纯度９７ ％ －
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| 关 键 词： | 固体超强酸 催化酯化 异戊氧基乙酸烯丙酯 香料 |
Synthesis of Allyl Isoamylglycolate by the Solid Superacid Catalyst TiO_2 /SO_4~(2-) |
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| YOU Yi,WANG Wen-feng,TANG Wei.Synthesis of Allyl Isoamylglycolate by the Solid Superacid Catalyst TiO_2 /SO_4~(2-)[J].Journal of Fuzhou University(Natural Science Edition),1999(5):88-90. |
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| Authors: | YOU Yi WANG Wen-feng TANG Wei |
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| Institution: | YOU Yi 1,WANG Wen-feng 1,TANG Wei 2 |
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| Abstract: | Allyl isoamylglycolate as perfume was prepared by isoamylglycolic acid and allyl alcohol in the presence of solid superacid catalyst TiO 2 /SO 2- 4 The influences of catalyst content, raw material ratio, reaction time on the yield of product were investigated The optimum synthetic conditions were estabished The yield of product reaches was 88 4%, and the purity is 97% |
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| Keywords: | solid superacid catalytic esterification allyl isoamylglycolate perfume |
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