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超顺磁性Fe3O4微粒的尺寸调控与磁性回收
引用本文:陈飞台,颜球辉,李晴,吴叶波,周彦成.超顺磁性Fe3O4微粒的尺寸调控与磁性回收[J].吉首大学学报(自然科学版),2016,37(5):19-22.
作者姓名:陈飞台  颜球辉  李晴  吴叶波  周彦成
作者单位:(1.College of Physics and Electromechanical Engineering,Jishou University,Jishou 416000, Hunan China;2.Key Laboratory of Mineral Cleaner Production and Exploitation of Green Functional Materials of Hunan Province,Jishou University,Jishou 416000,Hunan China)
基金项目:湖南省自然科学基金资助项目(2015JJ6093);吉首大学教学改革研究资助项目(2016008)
摘    要:以乙二醇为溶剂,通过温和的溶剂热法制备了具有不同颗粒尺寸大小的Fe3O4微米粒子.研究发现,通过调节反应体系中水、聚乙二醇-20000和铁离子的浓度,能有效控制Fe3O4的成核与生长,从而能实现对Fe3O4在较大颗粒尺寸范围内的有效调控.另外,相比小尺寸的Fe3O4,较大颗粒尺寸的超顺磁性粒子表现出更优良的磁性回收性能.由此可见,Fe3O4颗粒尺寸的有效调控对拓展其在纳米材料磁性回收中的应用具有非常重要的意义

关 键 词:.超顺磁性  Fe3O4  纳米材料  磁性回收  

Size-Controlled Synthesis and Magnetite Recovery of Superparamagnetic Fe_3O_4 Microparticles
CHEN Feitai,YAN Qiuhui,LI Qing,WU Yebo,ZHOU Yancheng.Size-Controlled Synthesis and Magnetite Recovery of Superparamagnetic Fe_3O_4 Microparticles[J].Journal of Jishou University(Natural Science Edition),2016,37(5):19-22.
Authors:CHEN Feitai  YAN Qiuhui  LI Qing  WU Yebo  ZHOU Yancheng
Institution:(1.College of Physics and Electromechanical Engineering,Jishou University,Jishou 416000, Hunan China;2.Key Laboratory of Mineral Cleaner Production and Exploitation of Green Functional Materials of Hunan Province,Jishou University,Jishou 416000,Hunan China)
Abstract:Fe3O4 microparticles of different size were synthesized by a novel solvothermal method,using ethylene glycol as solvent. It is found that the nucleation and growth of Fe3O4can be effectively controlled through adjusting the concentrations of water,polyethylene glycol 20000,and iron ion,which creates the possibility of controlling the size ofFe3O4 in a wide range effectively.Besides,Fe3O4 microparticle of larger size exhibits more excellent magnetic recycling property.As discussed above,the effective control ofFe3O4 particle is very important to expand its application in magnetite recovery of nanomaterials.
Keywords:superparamagnetism                                                                                                                        Fe3O4" target="_blank">3O4')">Fe3O4                                                                                                                        nanomaterials                                                                                                                        magnetite recovery
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