| 电化学法制备CuInSe2薄膜工艺的研究 |
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| 引用本文： | 徐玲,刘昌龄,吴世彪,陈少华,张信义,王利群,汪星和. 电化学法制备CuInSe2薄膜工艺的研究[J]. 合肥工业大学学报(自然科学版), 2006, 29(5): 547-550 |
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| 作者姓名： | 徐玲 刘昌龄 吴世彪 陈少华 张信义 王利群 汪星和 |
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| 作者单位： | 安徽建筑工业学院,材料科学与工程系,安徽,合肥,230022;安徽教育学院,化学系,安徽,合肥,230061 |
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| 摘 要： | 实验主要从基体材料的选择、络合剂的引用以及热处理试样等制备条件进行了初步的研究。通过分析与比较各种特定条件下制备出的试样的X射线衍射实验结果得知、导电玻璃作基体材料的镀层质量要比铜片和铁片的好;络合剂的加入有利于薄膜晶粒更加均匀和致密,可以改善镀层的质量;退火有利于薄膜晶粒的增大,使其结晶程度更好。
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| 关 键 词： | 电沉积 CuInSe2薄膜 X射线衍射分析 X射线光电子能谱 |
| 文章编号： | 1003-5060(2006)05-0547-04 |
| 修稿时间： | 2005-09-02 |
Research on preparing technology of CuInSe2 thin film by the electrochemical method |
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| XU Ling,LIU Chang-ling,WU Shi-biao,CHEN Shao-hua,ZHANG Xin-yi,WANG Li-qun,WANG Xing-he. Research on preparing technology of CuInSe2 thin film by the electrochemical method[J]. Journal of Hefei University of Technology(Natural Science), 2006, 29(5): 547-550 |
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| Authors: | XU Ling LIU Chang-ling WU Shi-biao CHEN Shao-hua ZHANG Xin-yi WANG Li-qun WANG Xing-he |
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| Abstract: | Three fundus materials on which the CuInSe2 thin film was electrodeposited were examined.The influence of the complex agent,that was added to the plating electrolyte,and annealing on the thin film was investigated.According to XRD analysis of the samples prepared under various conditions, the best fundus material is conductive glass;the citric acid as the complexing agent improves the plating quality and betters the uniformity and compactness of the thin film;and annealing enlarges the crystal grains of the thin film and improves the crystal degree. |
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| Keywords: | electrodeposition CuInSe_2 thin film XRD analysis X-ray Photoelectron Spectroscopy |
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