| 微波促进合成1-((1H-苯并[d]咪唑-2-氨基)甲基)-2-萘酚 |
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| 引用本文： | 李政,毛学荣.微波促进合成1-((1H-苯并[d]咪唑-2-氨基)甲基)-2-萘酚[J].西北师范大学学报,2010,46(3):63-66. |
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| 作者姓名： | 李政 毛学荣 |
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| 作者单位： | 西北师范大学化学化工学院,甘肃兰州,730070 |
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| 摘 要： | 在微波促进下,各种醛、β-萘酚、2-氨基苯并咪唑在无任何催化剂和溶剂的情况下,三组分一锅法合成了1-((1 H-苯并d]咪唑-2-氨基)甲基)-2-萘酚系列化合物.该方法具有反应时间短、操作简单、产率较高等特点.化合物的结构经过IR,1HNMR,13CNMR等得到证实.
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| 关 键 词： | 微波辐射 Mannich反应 2-氨基苯并咪唑 |
Microwave promoted synthesis of 1-((1H-benzo[d]imidazol-2-ylamino)methyl) naphthalen-2-ols |
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| LI Zheng,MAO Xue-rong.Microwave promoted synthesis of 1-((1H-benzo[d]imidazol-2-ylamino)methyl) naphthalen-2-ols[J].Journal of Northwest Normal University Natural Science (Bimonthly),2010,46(3):63-66. |
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| Authors: | LI Zheng MAO Xue-rong |
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| Institution: | LI Zheng,MAO Xue-rong(College of Chemistry , Chemical Engineering,Northwest Normal University,Lanzhou 730070,Gansu,China) |
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| Abstract: | A novel microwave-promoted three-component one-pot condensation reaction of an aldehyde,2-aminobenzod]imidazole and 2-naphthol under catalyst-free and solvent-free conditions to give 1-((1H-benzod]imidazol-2-ylamino)methyl)naphthalen-2-ols is described.This method has the advantages of short reaction time,simple manipulation and high yield.The structures of compounds are confirmed by IR,1HNMR,and 13CNMR. |
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| Keywords: | microwave irradiation Mannich reaction 1H-benzo[d]imidazol-2-amine |
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