A TEM study on the microstructure of spark plasma sintered ZrB_2-based composite with nano-sized SiC dopant

Sintering behavior of ZrB_2 ceramic with nano-sized SiC dopant was studied. ZrB_2-25 vol% nano-sized SiC was selected as the starting mixture to fabricate the composite. The manufacturing process was accomplished at 1800℃ for 5 min under 25 MPa via spark plasma sintering(SPS). The as-sintered sample reached a relative density of 99%. Besides the initial phases, namely ZrB_2 and SiC, the high-resolution X-ray diffraction(HRXRD) was used to study the formation of an in-situ ZrC phase. The possible chemical interactions during the ZrC phase formation were scrutinized. The microstructure of the composite was studied by the field emission scanning electron microscopy(FESEM) and transmission electron microscopy(TEM). Elemental analysis through FESEM evaluations revealed the formation of amorphous phases, rich in Zr, C, Si, B, and O elements, which was in harmony with the thermodynamical assessments. TEM studies endorsed the formation of such phases, containing a glassy bed of Si–B–O with ZrC and C islands dispersed therein.     

微波与生物组织的相互作用及微波理疗中若干实际考虑

本文论述了描述微波与生物组织相互作用的数学表达式,讨论工作频率选择、透入深度、反射、极化、泄漏及防护等实际问题。     

Mechanism of Microwave Effects on Conductivity of Solution

The relation between microwave conductivity and normal conductivity of solution is compared in this thesis. By building mathematical model and theoretical analyses, it indicates that the relationship of in situ conductivity of solution in microwave field and temperature is similar to that in non-microwave field. It can be expressed by quadratic equation but the values of both conductivities are different. Microwave field has effect on the mean path δ or hot vibrational frequency v of ions in solution. In microwave field, the mean energy barrier, which ions must surmount as they transit, is the function relation to temperature.     

棕榈油对淀粉物料微波膨化的影响

研究了棕榈油对淀粉物料微波膨化产品的质量和质构的影响。结果表明，棕榈油的添加减弱了微波的加热效果，且随着油含量的增加，温升速率逐渐减小，含油物料微波膨化过程中的加热段延长了10－20s，膨化段和固化段相应推迟10－20s，物料的膨化速度随着含油量的增加而减小。微波处理90s后，对照样及含油量为0.05,0.10,0.15和0.20mL/g的产品其膨化率分别为4.44,4.17,3.43,2.88和2.10。随着含油量的增加，产品的孔隙率逐渐增大，在含油量大于0.15mL/g后，这种增加程度加深，产品的质构变粗糙，向淀粉物料中添加棕榈油可以改善微波膨化产品的脆度，且在添加量为0.05mL/g时产品的硬度最小。添加棕榈油后的产品色泽与油含量有关，与微波膨化无关。     

微波辐射合成7-羟基-4-甲基香豆素

以浓硫酸为催化剂，采用微波辐射技术，由间苯二酚与乙酰乙酸乙酯缩合制备7－羟基－4－4甲基香豆素。结果表明，微波辐射合成7－羟基－4－4甲基香豆素的最以应条件为：间苯二酚5.5g，乙酰乙酸乙酯6.8ml，浓硫酸1.5ml，微波功率240W，微波辐射时间6min，产率84．1％，不采用微波辐射，反应时间大于10h，产率78％，红外光谱分析表明，7－羟基－4－4甲基香豆素的特征峰与7－羟基－4－甲基香豆素的各官能团的吸收峰吻合，测定7－羟基－4－甲基香豆素的熔点为189－192℃。     

一种减小反射式0－π调相器尺寸的新方法

在微波频率低端，按常规方法研制的调相器尺寸是大的，该文采用金属化孔和改变调整元件，结果证明，在不降低性能指标的情况下，可以减小调相器的尺寸。     

固定无线传输中的公务系统

讨论了固定无线传输干线上中、大容量数字微波系统中的公务系统，并研制了一种性能优于现有单话路系统的３话路公务系统。采用集成度高的开关电容滤波器，构成高阶分路滤波器；还提出了数字公务系统的构成、７０４ｋｂ／ｓ复接帧的帧结构及实现方案。     

制备泡沫铝的一种新方法:烧结溶解法

烧结溶解法是近几年发展起来的一种制造泡沫铝的新工艺，具有可以精确控制孔洞形状，尺寸和孔隙率及其分布等特点，具有较好的质量价格综合指数，是生产均匀或梯度微细开孔中密度泡沫铝的有效方法，所制泡沫铝在吸能，吸音等领域有广泛的应用前景。本文简要介绍烧结溶解法的原理与工艺，所制泡沫铝的组织特征与机械性能，并讨论与其它各类现有方法相比所具有的优势与局限。     

微波等离子体离子化检测器研究

本文采用氢气为载气和等离子体工作气体，以苯和二氧化碳为例，对不同电离电位样品组分经过和不经过等离子体两种样品引入检测器方式进行了详细的对比研究，发现检测器分别具有质量型和浓度型检测器的响应特征．探讨了空气引人等离子体对检测器分析性能的影响．     

Monitoring the sandstorm during spring season 2002 and desertification in northern China using SSM/I data and Getis statistics

A massive sandstorm enveloped most part of northern China during the spring season 2002. Monitoring the evolution of sandstorm and desertification has become one of the most serious problems for China's environment. Since 1989, one of the most advanced and operational passive microwave sensors is the DMSP SSM/I (special sensor microwave imager) operated at seven channels (19, 37, 85 GHz with the vertical and horizontal polarization and 22 GHz with vertical polarization only). In this paper, the sandstorm and desertification indexes, SDI and DI, are derived from the radiative transfer equation, and are employed with multi-channel measurements of the DMSP SSM/I for monitoring the sandstorm and desertification in northern China. Some SSM/I data in 1997 and 2001 are employed. The algorithm of Getis statistics is developed to categorize the spatial correlation and its evolution these days. It is demonstrated that the SSM/I indexes, SDI and DI, and its Getis statistics are well applicable for monitoring the sandstorm and desertification.