概率法在煤层气储量估算中的应用

煤层气田在勘探评价初期,储量估算参数往往存在一定的分布区间,采用体积法估算储量难以给出确定结果.针对此类问题,以M煤层气藏为例,利用概率法估算储量,围绕储量估算参数(储层面积、厚度、含气量),结合地质分析和储量参数样本分别建立理论分布模型(三角分布、正态分布、对数正态分布、威布尔分布、伽马分布)和任意分布模型;利用Kolmogorov-Smirnov(K-S)检验和卡方检验对相关理论分布模型进行拟合度优选;确立储层面积采用三角分布和正态分布模型,储层厚度采用威布尔分布和任意分布模型,储层含气量采用伽马分布和任意分布模型,并形成4组不同模型组合方案,再利用蒙特卡罗方法对储量进行估算.结果表明:任意分布模型服从原始样本分布,置信区间较窄,理论分布模型则体现过滤作用,两者对储量估算结果有一定影响;储层含气量对储量估算结果影响较大;概率法可以排除人为因素,估算出不同概率级别下的储量,从而起到降低决策风险的作用.     

模具结构对连续纤维增强热塑性复合材料性能的影响

采用自行设计的两种不同结构的熔融浸渍模具制备了连续玻璃纤维增强聚丙烯预浸带，测试了模具结构对预浸带的孔隙率、纤维断裂率、界面形貌、纤维分散均匀度和拉伸强度的影响，建立了纤维浸渍模型和纤维断裂模型，并通过理论模型对预浸带的孔隙率和断裂率进行理论预测。结果表明，本文建立的数学模型能够有效预测预浸带的浸渍程度和纤维断裂率，可用于浸渍模具结构的优化设计；在本文范围内，与波浪形模具相比，斜齿形模具的多楔形区结构可以有效地降低预浸带孔隙率和提升纤维分散程度；波浪形模具的流道圆角半径较大，楔形区个数较少，与斜齿形模具相比，可有效降低纤维断裂率并提升拉伸性能。     

一种基于智能手机的动态血压监测仪设计与实现

以嵌入式STM 32芯片为核心,设计了一种人体血压动态监测仪.设备包括采集电路、驱动电路、显示电路、蓝牙、微信小程序等模块,可通过智能手机上的微信小程序界面实时显示人体心率、舒张压和收缩压等数据,实现对血压敏感人群血压状态的动态监测和历史数据查询.     

黄体酮缓释栓剂的制备与优化

以热熔法制备黄体酮缓释栓剂,转篮法考察栓剂的体外溶出效果,并采用高效液相色谱法测定黄体酮的含量,筛选栓剂基质以及优化释放速度调节剂浓度.实验结果表明:以混合脂肪酸甘油酯作为栓剂基质制备的黄体酮缓释栓剂能保留50 h的完整形态;羟丙基甲基纤维素、羧甲基纤维素钠和硬脂酸3种释放速度调节剂的最佳浓度分别为1.5%、0.5%、1%,其中,以1%的硬脂酸为释放速度调节剂制备的黄体酮缓释栓剂在48h时的药物溶出度为73.90%,其释药时间超过50 h,缓释效果优于羟丙基甲基纤维素、羧甲基纤维素钠.     

Improved hemimorphite flotation using xanthate as a collector with S(Ⅱ) and Pb(Ⅱ) activation

The flotation of hemimorphite using the S(Ⅱ)–Pb(Ⅱ)–xanthate process,which includes sulfidization with sodium sulfide,activation by lead cations,and subsequent flotation with xanthate,was investigated.The flotation results indicated that hemimorphite floats when the S(Ⅱ)–Pb(Ⅱ)–xanthate process is used; a maximum recovery of approximately 90% was obtained.Zeta-potential,contact-angle,scanning electron microscopy–energy-dispersive spectrometry(SEM–EDS),and diffuse-reflectance infrared Fourier transform spectroscopy(DRIFTS) measurements were used to characterize the activation products on the hemimorphite surface and their subsequent interaction with sodium butyl xanthate(SBX).The results showed that a Zn S coating formed on the hemimorphite surface after the sample was conditioned in an Na2 S solution.However,the formation of a Zn S coating on the hemimorphite surface did not improve hemimorphite flotation.With the subsequent addition of lead cations,Pb S species formed on the mineral surface.The formation of the Pb S species on the surface of hemimorphite significantly increased the adsorption capacity of SBX,forming lead xanthate(referred to as chemical adsorption) and leading to a substantial improvement in hemimorphite flotation.Our results indicate that the addition of lead cations is a critical step in the successful flotation of hemimorphite using the sulfidization–lead ion activation–xanthate process.     

Bidirectional Feedback Dynamic Particle Filter with Big Data for the Particle Degeneracy Problem

Particle Filter(PF) is a data assimilation method to solve recursive state estimation problem which does not depend on the assumption of Gaussian noise, and is able to be applied for various systems even with non-linear and non-Gaussian noise. However, while applying PF in dynamic systems, PF undergoes particle degeneracy,sample impoverishment, and problems of high computational complexity. Rapidly developing sensing technologies are providing highly convenient availability of real-time big traffic data from the system under study like never before. Moreover, some sensors can even receive control commands to adjust their monitoring parameters. To address these problems, a bidirectional dynamic data-driven improvement framework for PF(B3 DPF) is proposed.The B3 DPF enhances feedback between the simulation model and the big traffic data collected by the sensors,which means the execution strategies(sensor data management, parameters used in the weight computation,resampling) of B3 DPF can be optimized based on the simulation results and the types and dimensions of traffic data injected into B3 DPF can be adjusted dynamically. The first experiment indicates that the B3 DPF overcomes particle degeneracy and sample impoverishment problems and accurately estimates the state at a faster speed than the normal PF. More importantly, the new method has higher accuracy for multidimensional random systems.In the rest of experiments, the proposed framework is applied to estimate the traffic state on a real road network and obtains satisfactory results. More experiments can be designed to validate the universal properties of B3 DPF.     

不同产地独活及其混伪品的质量差异性分析

多点采样,对不同来源的独活及其混伪品进行质量差异性分析.测定不同产地独活及其混伪品总灰分、酸不溶性灰分、蛇床子素和二氢欧山芹醇当归酸酯质量分数,并结合HPLC指纹图谱对不同产地独活及其混伪品开展质量评价.结果表明,不同产地独活除陕西样品的蛇床子素略低于《中华人民共和国药典》(以下简称《药典》)标准外,其余样品均符合《药典》质量要求,而独活混伪品的蛇床子素质量分数均远低于正品独活质量分数.不同产地的独活HPLC指纹图谱有25个共有峰,各独活样品的指纹图谱与对照图谱的相似度在0.9以上,所建立的指纹图谱可用于独活的质量评价.因此,多指标的测定结果结合HPLC指纹图谱,可有效对不同产地的独活质量进行差异性分析和评价;混伪品蛇床子素的质量分数远低于正品独活,蛇床子素的质量分数高低可作为正品独活区别于混伪品的一个重要特征指标.     

一种基于虚拟传感的双通道主动降噪方法

在主动噪声控制系统中,有效降噪范围受通道数量的影响很大,传统方式主要是通过增加系统通道数量来扩大有效降噪范围(3 dB以上),成本较高,且对计算能力要求极高.为实现在不增加通道数、误差传感器及扬声器数量的情况下,扩大有效降噪范围,使用了一种基于虚拟误差传感的方法,在FxLMS双通道主动噪声控制系统中研究虚拟传感器设置的位置与有效降噪范围的关系.结果表明:在虚拟传感器设置为不同位置时,有效降噪范围由12 cm增加到26 cm.