高温涂层自愈合性能的研究

探讨了用涂层的高温透气性的变化率评价涂层自愈合性的实验方法，研究了涂层高温自愈合能力的可能性，并用该方法研究了玻璃质涂层的高温自愈合性能．     

硫酸钡改性新型甲基化环糊精毛细管色谱柱柱行为的研究

在硫酸钡微晶对毛细管内壁改性的基础上,系统制备了甲基环糊精与不同混合固定液的毛细管色谱柱,从柱的分离选择性,惰性,柱效和分析准确性等方面作了较为系统的研究,并对环糊精的分离机理作了初步探索。     

神经网络高炉铁水含硅量预报模型

研究了基于神经网络的高炉铁水含硅量预报模型，运用高炉生产过程中工艺参数，实现了铁水含硅量的中短期预报，仿真结果表明，本模型具有良好的预报效果。     

渗铸法生产泡沫铝合金的模具设计参数的确定

设计了一套适合制造小孔径泡沫铝合金的渗铸装置，并且生产出了泡沫铝试样．确定了铸型的结构形式和压头与压空间的间隙值，以及铸型所用的涂料，并确定了铸型的最小壁厚．分析了铸型在压渗时存在的应力，指出模具所受切向压力是引起模具破坏的主要力，适当增加壁厚可保证模具在压渗铝合金时不被胀形和弯曲．探讨了食盐粒子的预处理工艺．散状粒子的预处理工艺是将食盐粒子加热至４５０℃，并保温９０～１２０ｍｉｎ．     

磁性壳聚糖微球的表征及其磁响应性

以戊二醛为交联剂、Fe3O4为磁核,采用反相悬浮交联技术合成了磁性壳聚糖微球,并利用数码光学显微成像仪、激光粒度仪、傅立叶红外光谱对磁性微球的形态、大小和化学结构进行了表征,采用原子吸收分光光度仪、磁天平和可调磁场对其磁响应性进行了研究.结果表明:所合成的磁性壳聚糖微球粒径在50~200μm之间,基本呈圆球形,表面比较光滑,且内部均匀分布着磁性介质Fe3O4;当磁性微球粒径小于280μm时,在外加磁场作用下,微球的磁化率与沉降速度都随着微球粒径的增大而增大.这表明所制备的磁性壳聚糖微球具有良好的磁响应性.     

镍(Ⅱ)和铜(Ⅱ)配合物的氧化还原与pH值相关性的研究

用循环伏安法研究了两个新的三元配合物[Ni(phendio)(TPA)](CIO_4)_2(1)和[Cu(phendio)(TPA)] (CIO_4)_2(2)(phendio=1,10-菲咯啉-5,6-二酮,TPA=三(2-吡啶甲基)胺)在pH 2～9的磷酸盐缓冲溶液中的电化学性质．实验结果表明,在-0．3～0．4 V(vs．SCE)电位扫描范围内这两个配合物都表现出与pH值相关的氧化还原活性,pH＜4时,是2e~-/3H~ 过程,pH＞4时为2e~-/2H~ 过程．     

植物马桑中挥发油成分的GC-MS分析

利用水蒸气蒸馏法提取马桑叶和茎中的挥发油,并采用气-质联用(GC-MS)方法对挥发油中化学成分进行分析.鉴定出了马桑叶和茎中的挥发油成分中的20及26种化合物,马桑叶挥发油中所鉴定出的主要成分为二苯胺和邻苯二甲酸异丁酯,含量分别为10.22%和10.07%.马桑茎挥发油中鉴定出的主要成分也为二苯胺和邻苯二甲酸异丁酯,但含量与马桑叶中不同,分别为1.61%和1.05%.     

中立型随机时滞微分方程的离散反馈镇定

考虑了中立型随机时滞微分方程基于离散时间状态观测的反馈镇定问题.首先建立了受控系统均方指数稳定的充分条件,然后基于此用线性矩阵不等式方法设计了所需的离散时间的反馈控制器,最后举例说明了所得结果的有效性.     

Mechanical characterization and strain-rate sensitivity measurement of Ti- 7333 alloy based on nanoindentation and crystal plasticity modeling

The relationship between crystal orientations and meso-mechanical properties of β phase Ti-7333 titanium was investigated through the combination of nanoindentation experiments and simulation. The crystal plasticity finite element(CPFE) model for nanoindentation of single body-centered cubic crystal was established based on the experimental data. And the crystal plasticity constitutive law was implemented to simulate the nanoindentation process, obtaining satisfied results with an acceptable error. From the simulated pileup morphology patterns with different crystal orientations, it was found that the β phase experienced a symmetrical and orientation-related deformation process. Meanwhile, the strain-rate sensitivity(SRS) of β phase was investigated through nanoindentation tests based on continuous stiffness measurement(CSM) under different strain rates,varying between 0.2, 0.05 and 0.01 s~(-1). Two grains with different orientations exhibited similar SRS exponents,m, calculated from the experimental results.     

Products Ranking Through Aspect-Based Sentiment Analysis of Online Heterogeneous Reviews

With the rapid growth of online shopping platforms, more and more customers intend to share their shopping experience and product reviews on the Internet. Both large quantity and various forms of online reviews bring difficulties for potential consumers to summary all the heterogenous reviews for reference. This paper proposes a new ranking method through online reviews based on different aspects of the alternative products, which combines both objective and subjective sentiment values. Firstly, weights of these aspects are determined with LDA topic model to calculate the objective sentiment value of the product. During this process, the realistic meaning of each aspect is also summarized. Then, consumers’ personalized preferences are taken into consideration while calculating total scores of alternative products. Meanwhile, comparative superiority between every two products also contributes to their final scores. Therefore, a directed graph model is constructed and the final score of each product is computed by improved PageRank algorithm. Finally, a case study is given to illustrate the feasibility and effectiveness of the proposed method. The result demonstrates that while considering only objective sentiment values of the product, the ranking result obtained by our proposed method has a strong correlation with the actual sales orders. On the other hand, if consumers express subjective preferences towards a certain aspect, the final ranking is also consistent with the actual performance of alternative products. It provides a new research idea for online customer review mining and personalized recommendation.