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排序方式: 共有7492条查询结果,搜索用时 15 毫秒
1.
Cobalt (Co)-modified brownmillerite KBiFe2O5 (KBFO; [KBiFe2(1?x)Co2xO5 (x = 0, 0.05)]) polycrystalline is synthesized following the solid-state reaction route. Rietveld refinement of X-ray diffraction data confirmed the phase purity of KBFO and KBiFe1.9Co0.1O5 (KBFCO). The optical bandgap energy (Eg) of KBFO decreased from 1.59 to 1.51 eV because of Co substitution. The decrease in bandgap can be attributed to the tilting of the Fe–O tetrahedral structure of KBFCO. The observed room-temperature Raman peaks of KBFCO shifted by 3 cm?1 toward a lower wavenumber than that of KBFO. The shift in Raman active modes can be attributed to the change in the bond angles and bond lengths of the Fe–O tetrahedral structure and modification in response to oxygen deficiency in KBFO because of Co doping. Compared with that of KBFO, the frequency-dependent dielectric constant and dielectric loss of KBFCO decrease at room temperature, which is a con-sequence of the reduction in oxygen migration and modification in response to vibrational modes present in the sample. 相似文献
2.
The effect of cold rolling and post-rolling heat treatment on the microstructural and electrochemical properties of the 316L stainless steel was investigated.Two-pass and four-pass cold-rolled stainless steel specimens were heat-treated by annealing at 900℃followed by quenching in water.During the cold rolling,the microstructure of the as-received specimen transformed from austenite to strain-inducedα′-martensite due to significant plastic deformation that also resulted in significant grain elongation(i.e.,~33%and 223%increases in the grain elongation after two and four rolling passes,respectively).The hardness of the heat-treated as-received specimen decreased from HV 190 to 146 due to the recovery and recrystallization of the austenite grain structure.The cyclic polarization scans of the as-rolled and heat-treated specimens were obtained in 0.9wt%NaCl solution.The pitting potential of the four-pass rolled specimen was significantly increased from 322.3 to 930.5 mV after post-rolling heat treatment.The beneficial effect of the heat treatment process was evident from~10-times-lower corrosion current density and two-orders-of-magnitude-lower passive current density of the heat-treated specimens compared with those of the as-rolled specimens.Similarly,appreciably lower corrosion rate(3.302×10?4mm/a)and higher pitting resistance(1115.5 mV)were exhibited by the postrolled heat-treated specimens compared with the as-rolled 316L stainless steel specimens. 相似文献
3.
For this study, we synthesized Aurivillius Bi5Ti3FeO15 ceramic using the generic solid-state reaction route and then performed room-temperature X-ray diffraction to confirm that the compound had a single phase with no impurities. The surface morphology of the prepared sample was observed to contain microstructural grains approximately 0.2–2 μm in size. The dielectric properties of the sample were determ-ined as a function of frequency in a range of approximately 100 Hz to 1 MHz at various temperatures (303 K ≤ T ≤ 773 K). Nyquist plots of the impedance data were found to exhibit a semi-circular arc in the high-temperature region, which is explained by the equivalent electrical circuit (R1C1)(R2QC2), where R1 and R2 represent the resistances associated with the grains and grain boundaries, respectively, C1 and C2 are the re-spective capacitances, and Q is the constant phase element (CPE), which accounts for non-Debye type of behavior. Our results indicate that both the resistance and capacitance of the grain boundaries are more prominent than those of the grains. The alternating current (ac) conductiv-ity data were analyzed based on the Jonscher universal power law, which indicated that the conduction process is dominated by the hopping mechanism. The calculated activation energies of the relaxation and conduction processes were very similar (0.32 to 0.53 eV), from which we conclude that the same type of charge carriers are involved in both processes. 相似文献
4.
5.
基于百度指数平台,获取了2011年、2013年及2015年我国大陆31个省、直辖市和自治区的新疆旅游搜索指数.运用季节集中指数、周内分布偏度指数、空间自相关方法对新疆旅游关注度的时空差异进行了分析并引入GWR模型探究其影响因素.结果表明:(1)新疆旅游关注度总体呈现增长态势,且各年关注度表现出明显的季节性特征,节假日、周存在"前兆效应";(2)全国各省、直辖市和自治区的新疆旅游关注度具有显著的空间自相关性,大多数地区呈现出持续的"低—低"集聚现象;(3)GWR模型优于OLS模型,从全域视角看,人口规模、经济发展水平、教育发展水平及互联网发展水平对新疆旅游关注度的影响均呈现不同程度的正向作用;从局域视角看,各影响因素作用整体上与OLS模型结果一致,但各影响因素的敏感度在空间上表现出西部地区高于东部地区的态势. 相似文献
6.
基于2008-2017年江西省历次启动自然灾害救助应急响应的统计数据,分析研究了江西省自然灾害救助应急响应的时空分布变化规律和特征。结果表明:1)江西省是一个自然灾害多发频发的省份,近10 a启动救助应急响应58次,平均每年要应对近6次重大自然灾害;2)洪涝灾害是江西省自然灾害的主要灾种,近10a针对洪涝灾害启动响应42次、占总数的72%。启动响应依据指标最多的是紧急转移安置人口、其次是因灾死亡人口;3)启动应急响应时间基本在5-8月份,6月份又是最多的月份,表明重特大自然灾害主要发生在5-8月份;4)启动救助应急响应总次数呈现出北部多、南部少的地域分布特征。 相似文献
7.
Y.Pazhuhanfar B.Eghbali 《矿物冶金与材料学报》2021,28(6):1080-1089
In the present research, aluminum metal matrix composites were processed by the stir casting technique. The effects of TiB2 rein-forcement particles, severe plastic deformation through accumulative roll bonding (ARB), and aging treatment on the microstructural charac-teristics and mechanical properties were also evaluated. Uniaxial tensile tests and microhardness measurements were conducted, and the micro-structural characteristics were investigated. Notably, the important problems associated with cast samples, including nonuniformity of the rein-forcement particles and high porosity content, were solved through the ARB process. At the initial stage, particle-free zones, as well as particle clusters, were observed on the microstructure of the composite. However, after the ARB process, fracturing phenomena occurred in brittle ceramic particles, followed by breaking down of the fragments into fine particles as the number of rolling cycles increased. Subsequently, com-posites with a uniform distribution of particles were produced. Moreover, the tensile strength and microhardness of the ARB-processed com-posites increased with the increase in the reinforcement mass fraction. However, their ductility exhibited a different trend. With post-deforma-tion aging treatment (T6), the mechanical properties of composites were improved because of the formation of fine Mg2Si precipitates. 相似文献
8.
体温通常用于筛查传染病、监测治疗.为了确定皮肤表面温度.通过恒压式测温电路测电阻的方法,研究设计了可穿戴式多点体温监测系统,以STM32F103C8T6芯片为核心处理器,负温度系数热敏电阻(negative temperature coefficient,NTC)作为感温元器件,ADS1256芯片为温度信号调理器,蓝牙模块为无线传输单元,用LABVIEW设计上位机界面.热敏电阻及分压电阻构成的恒压式电桥电路进行8路温度数据的采集,24bits超高精度模数转换模块配置差分输入对模拟信号进行放大、滤波以及模数转换;转换后的数据在单片机中处理和运算;最终通过蓝牙将数据传至上位机.采用Stein-hart方程的四阶公式对热敏电阻作线性补偿.从软件和硬件上减少环境干扰和体温分布不均的影响.分析了温传感器的温度测量误差.实验结果表明,测量系统分辨率达0.01℃,测温准确度可达±0.02℃.此设计方案,具有较高的稳定性和精确性;并且该电路结构简单、体积小、低功耗,可用于需要精密测体温场合. 相似文献
9.
Aluminum alloy matrix composites have found a predominant place in research, and their applications are explored in almost all industries. The aerospace industry has been using precipitation-hardenable alloys in structural applications. However, insufficient literature is available on the influence of multiwalled carbon nanotubes (MWCNTs) on precipitation-hardenable alloy composite materials; thus, this work was designed to elucidate the effect on MWCNT reinforcement on AA2219 with and without precipitation hardening. Reinforcement with MWCNTs has been reported to accelerate precipitation and to achieve greater hardness within a much shorter time. The addition of 0.75wt% MWCNTs resulted in maximal hardness at 90 min, which is approximately 27% of improvement over the maximum hardness achieved by the corresponding monolithic alloy after 10 h of aging. The sample reinforced with 0.75wt% MWCNTs showed an improvement of 82% in hardness by solutionizing and aging compared to that achieved by sintering. 相似文献
10.
通过检测高尿酸血症大鼠血清代谢谱的变化,探讨代谢组学在高尿酸血症研究中的应用。将20只清洁级健康SD(Sprague-Dawley)大鼠随机分为高尿酸血症模型组(10只)和空白对照组(10只),每日采用酵母膏(YEP)21 g·kg-1·d-1给予喂养,氧氢酸钾(OA)以200 mg-1·kg-1·d-1腹腔注射1次,建立高尿酸血症大鼠模型。第28日收集空白对照组和模型组大鼠血清,进行1H-NMR谱测定和主成分分析。与空白对照组大鼠相比,模型组大鼠血清中糖蛋白、丙酮酸、丙氨酸、异亮氨酸、亮氨酸显著增加,而甲酸浓度及极低密度脂蛋白、不饱和脂肪酸、丙酮显著降低。由此得出,高尿酸血症大鼠血清代谢组学发生明显变化,血浆代谢组学在一定程度上反映高尿酸血症大鼠的病理生理变化。 相似文献