微波加热内配碳酸钙高碳铬铁粉固相脱碳

高碳铬铁无渣脱碳法可避免有毒铬渣的排放,利用微波场可快速加热粉状物料的特性,在高碳铬铁粉中配加一定比例的碳酸钙粉,可实现高碳铬铁粉快速固相脱碳.实验结果表明:配加一定比例的碳酸钙粉,不会影响内配碳酸钙高碳铬铁粉混合物料的微波加热特性;提高混合物料的脱碳摩尔比、微波加热温度和保温时间,有利于高碳铬铁粉的深度脱碳,但相应加剧脱碳铬铁粉的氧化程度.合适的固相脱碳条件为:脱碳摩尔比1∶1.0~1∶1.4,微波加热温度1100℃,保温脱碳时间60 min.在上述条件下可使碳质量分数为8.16%的高碳铬铁粉脱碳至3.91%~1.71%,脱碳率为52.08%~79.04%.     

高能炸药的X射线及γ射线探测安全性研究

为解决X射线、γ射线探测技术在高能炸药属性、状态特征测量中的应用安全性疑虑,提高检测速度,采用了常用工程应用数学指标,分别从单个高能炸药分子与光子的作用几率和高能炸药对光子能量的吸收角度,得到了采用X射线、γ射线探测高能炸药属性、状态特征时的辐照强度阈值. 研究结果表明,目前工业常用的辐射探测方法可以安全地应用于高能炸药,且在确保量级不大于104 W/m2时,可安全地进一步提高高能炸药的辐照强度.      

皮带巷电机暂态过程对电磁环境的影响

利用ATP软件仿真皮带电机暂态过程,并运用传输线模型分析瞬态脉冲沿巷道和电缆的衰减特性. 结果表明,理论上电机起动、制动及负载突变时产生的瞬态脉冲电压峰值最大为额定电压的6倍,电流峰值最高可达额定电流的11倍;瞬态辐射发射对皮带巷电磁环境的影响较小,而瞬态脉冲沿长电缆传播会产生较大衰减. 确定煤矿井下现场测量工具及测点布置方法,分析比较实测数据与理论值,结果说明皮带电机起动和制动过程产生的瞬态辐射骚扰可以忽略,瞬态传导骚扰较大,但脉冲峰值最大不会超过额定值的4倍. 提出的井下现场测量方法、获得的实测数据和理论值为矿井电磁兼容性研究提供了参考依据.      

Novel laminated multiferroic heterostructures for reconfigurable microwave devices

Voltage tuning of magnetism is fundamentally and technically important for fast, compact and ultra-low power electronic devices. Multiferroic heterostructures,simultaneously exhibiting distinct ferroelectric and ferromagnetic properties, have caught a lot of attentions because of the capability of controlling magnetism by a voltage via a strain-mediated magnetoelectric（ME） coupling. In these materials, a voltage-induced strain is involved to create an effective magnetic field and change ferromagnetic resonance frequency in the coupled ferromagnetic phases through magnetoelastic interactions. Therefore, the devices made of such materials are compact, ultra-fast and energy efficient,providing new functionalities for microwave components.This paper will review the recent progress of multiferroics and their applications in microwave devices from different aspects, including the creation of the novel laminated multiferroic heterostructures with a strong ME coupling, the realization of the multiferroics based on tunable microwave signal processors and the investigation of nonvolatile tuning of microwave properties using ferroelastic domain switching in multiferroic heterostructures. These tunable multiferroic heterostructures and devices offer great opportunities for realizing the next generation of tunable magnetic microwave components, ultra-low power electronics and spintronics.     

Constructal entransy optimizations for insulation layer of steel rolling reheating furnace wall with convective and radiative boundary conditions

Based on the entransy dissipation extremum principle for thermal insulation process, the constructal optimizations for a plane insulation layer of the steel rolling reheating furnace wall with convective and radiative boundary conditions are carried out by taking the minimization of entransy dissipation rate as optimization objective. The optimal construct of the plane insulation layer is obtained. The results show that for the convective heat transfer boundary condition, the optimal constructs of the insulation layer obtained based on the minimizations of the entransy dissipation rate and heat loss rate are obvi- ously different. Comparing the optimal construct obtained based on the minimization of the entransy dissipation rate with that based on the minimization of the heat loss rate, the entransy dissipation rate is reduced by 5.98 %, which makes the global thermal insulation performance of the insulation layer improve. For the combined convective and radiative heat transfer boundary condition, compared the insulation layer having an increasing thickness with that having constant thickness and a decreasing thickness, the entransy dissipation rates are reduced by 16.59 % and 39.72 %, respectively, and the global thermal insulation performance of the insulation layer is greatly improved.There exits an optimal constant coefficient α2,opt which leads to the minimum dimensionless entransy dissipation rate of the insulation layer. The difference between the optimal constant coefficients α2,opt obtained based on the minimizations of the entransy dissipation rate and the maximum temperature gradient of the insulation layer is small. This makes the corresponding thermal stress obtained based on the minimum dimensionless entransy dissipation rate also be small, and the global thermal insulation performance and thermal safety of the insulation layer are improved simultaneously. The results obtained can provide some guidelines for the optimal designs of the insulation layers.     

星用镀膜光学透镜空间带电粒子辐射效应评价

针对K509玻璃基镀膜透镜空间带电粒子辐射效应,使用两种能量的电子和60 Coγ射线作为模拟源进行了辐照试验,并分析了辐照效应与轨道带电粒子辐射的差别.在此基础上,提出了一种针对镀膜光学透镜,使用低能电子和60 Coγ射线接续辐照,模拟空间带电粒子辐射效应的试验方法.     

电源通过GJB151A-97标准测试实例

<正>0引言目前大多数电子产品都选用开关电源供电,以节省能源和提高工作效率,按照电源的规范要求制造的电源是不应该有干扰的。但由于设计时对EMC问题没有严格的规范要求或执行不力,设计人员也就没有对电源的EMC问题做深入细致的研究,导致开关电源是目前电子产品中最主要的电磁干扰源之一,这也是国内目前的现状。当一个系统出现干扰问题时,人们首先是找电源的问题,以至有"电源时干扰之源"之说。电源干扰的原因有多种,一是干扰原因较多,二是干扰能量较大,三是干扰频带较宽。理想的电源应该是从电路设计开始就进行EMC设计。     

微波-超声波辅助提取金丝小枣环磷酸腺苷的技术研究

为提高金丝小枣环磷酸腺苷提取率,以金丝小枣为原料,通过Plackett-Burman(PB)实验设计,确定了影响金丝小枣环磷酸腺苷提取率的显著因素为微波时间、料液比、超声时间和超声功率。在此基础上,通过Box-Behnken(BB)实验设计、响应面分析法,最终得出了超声时间是影响提取效果的最显著因子,其次是料液比,微波时间、超声功率在设定条件范围内对提取效果影响不显著。确定了金丝小枣环磷酸腺苷的最佳提取条件为微波功率440 W、微波时间64 s、料液比1:8、超声时间21 min、超声功率300 W、超声温度20℃,在此条件下,金丝小枣环磷酸腺苷提取率为90.83%。本研究成果能够为医药和食品工业提供良好的天然活性物质,为金丝小枣及其他枣品的深加工和工业化应用提供了参考依据。     

含1,2,4-三唑希夫碱结构的6-取代吲哚衍生物的微波合成及其抗菌活性研究

在微波辐射条件下,以吲哚-6-甲酸甲酯为原料,设计合成了8个含1,2,4-三唑结构单元的希夫碱型吲哚衍生物.通过微波法和常规法的研究对比发现,使用微波法后,产率从54%~72%提高到75%~92%,反应时间从80~120分钟缩短到8~10分钟.所有化合物的结构经1H NMR,IR,ESI-MS及元素分析确证.初步的抗菌活性表明,化合物5b和5c分别对大肠杆菌和金黄色葡萄球菌有一定的抑制作用.     

功能化PVDC负载钯配合物在微波促进下催化Suzuki反应

聚偏二氯乙烯(PVDC)被二乙烯三胺(DETA)修饰后可以有效负载氯化钯,从而制得催化剂PVDC-DETA-Pd.利用IR、TG、XPS等测试手段对其结构进行了表征.热分析表明,催化剂在室温至200℃有很好的热稳定性.该催化剂在微波促进条件下有良好的催化性能,可以催化各种芳基卤化物和四苯硼钠间的Suzuki反应.并且催化剂回收再利用5次后,产率仍能达到75%.