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991.
以二(碘乙基)醚与4,5.二氰乙硫基-1,3.二硫杂环戊烯-2-硫酮为起始原料,采用氰乙基保护与脱保护技术,通过多步缩合反应以较好的收率合成了含4个1,3.二硫杂环戊烯-2-硫酮并硫杂36冠-12(5),给出了目标化合物的有效合成方法,并用1HNMR,MS和EA对其进行了表征. 相似文献
992.
Introduction During development, many cell types exhibit sponta-neous neurotransmitter release, with synaptic transmis-sions crucial for normal nervous system activity. Syn-aptic transmissions are initiated when an action poten-tial triggers the neurotran… 相似文献
993.
WANG Danghui YANG Yixin YANG Yiqin ZHAO Tiancheng WU Xing WANG Shaokang HOU Yao CHEN Weizong 《科学通报(英文版)》2006,51(7):785-790
Abstract The 2-acetyl-benzimidazoledehyde-glycine Schiff-base ligand and the corresponding Pr(Ⅲ) complex Pr2L3(NO3)3· 2CH3OH (L=C11H10N3O2) were synthesized in methanol and characterized by a series of methods, including chemical analysis, elemental analysis, TOF-MS, ^1H NMR, UV-, IR-, Raman spectra, thermal analysis, and the three-dimension fluorescence excitation and emission spectra. The Pr(Ⅲ) complex exhibits extraordinary water-solubility and the Pr(Ⅲ) hydroxide appears at pH≥13. The complex also possesses specific fluorescent properties. Thus, at the excitation wavelengths 200.0-280.0 and 260-350 nm the fluorescence bands were observed at 290.0 and 400.0 nm, respectively. 相似文献
994.
Differences between dynamics factors for interannual and decadal variations of rainfall over the Yangtze River valley during flood seasons 总被引:4,自引:0,他引:4
PING Fan LUO Zhexian JU Jianhua 《科学通报(英文版)》2006,51(8):994-999
The prediction of rainfall in the Yangtze River valley, especially, during flood seasons is the main means for scientists in China working on and the understanding of rainfall-associated processes is a crucial component of this effort. It can be derived f… 相似文献
995.
Global warming: Take action or wait? 总被引:1,自引:0,他引:1
W.S.Broecder 《科学通报(英文版)》2006,51(9):1018-1029
Of all the changes wrought by human activity, the buildup in our atmosphere of the greenhouse gases, carbon dioxide, methane and nitrous oxide, has gener- ated the most contentious debate. Environmentalists warn that in the absence of firm action, over th… 相似文献
996.
Photocatalytic degradation of trace-level of MicrocystinLR by nano-film of titanium dioxide 总被引:1,自引:0,他引:1
FENG Xiaogang RONG Fei FU Degang YUAN Chunwei HU Yan 《科学通报(英文版)》2006,51(10):1191-1198
The occurrence of toxic water bloom of cyanobacte-ria algae, widely reported in eutrophic freshwater, hasbeen a serious pollution problem in recent years[1]. Mi-crocystins (MCs), the most common cyanobacteriatoxin with a cyclic heptapeptide structure (Fig… 相似文献
997.
CHANG Qihai YANG Guotao SONG Juan GONG Shunsheng 《科学通报(英文版)》2006,51(21):2657-2661
The stability of the middle atmosphere ranging from 30 km to 60 km over Wuhan is elementarily studied, according to the observational data obtained in about one year through the WlPM Rayleigh lidar. The stability parameter (buoyancy frequency squared), which was obtained through the temperature field, shows that the middle atmosphere over Wuhan is stable all the year round, but the stability appears variable because the stability of summer and winter is lower, and that of spring and autumn is higher. 相似文献
998.
CHEN Zhen YANG Juekuan ZHUANG Ping CHEN Minhua ZHU Jian CHEN Yunfei 《科学通报(英文版)》2006,51(23):2931-2936
The thermal conductivities of InGaAs/ InGaAsP superlattices with different period lengths were measured from 100 to 320 K using 3ω method. In this temperature range, the thermal conductivities were found to decrease with an increase in temperature. For the period length-dependant thermal conductivity, the minimum value does exist at a certain period length, which demonstrates that at a short period length, superlattice thermal conductivity increases with a decrease in the period length. When the period is longer than a certain period length, the interface thermal resistance dominates in phonon transport. The experimental and theoretical results confirmed the previous predictions from the lattice dynamics analysis, i.e. with the increase in period length, the dominant mechanisms of phonon transport in superlattices will shift from wave mode to particle mode. This is crucial for the cutoff of the phonons and lays a sound foundation for the design of superlattice structures. 相似文献
999.
右江革命根据地时期的红色歌谣初探 总被引:1,自引:0,他引:1
简华春 《广西右江民族师专学报》2006,19(2):51-55
右江革命根据地建设时期,右江军民通过音乐手段来推广革命道理,创作了数量众多、内容丰富、题材广泛的红色歌谣.他们用流行的革命歌曲、民歌、民谣等形式在圩场、会议、学校通过教唱、对歌、演唱、传唱的方式控拆黑暗社会、发动民众,讴歌农民运动及战斗生活,赞美苏维埃建设,表达了右江民众热爱党、热爱红军和积极参加革命的朴素情感,具有明显的革命教育和文化传播作用. 相似文献
1000.
Hg~(2+)与NBS修饰前后两种血清蛋白结合的研究(英文) 总被引:2,自引:2,他引:2
外加毫摩尔浓度的重金属离子Hg2+,会引起BSA或HSA的色氨酸荧光下降,并且35℃时的变化比25℃时更明显,HSA的变化比BSA的大.SternVol mer作图分析结果表明荧光淬灭主要是由动态淬灭引起的.用NBS对BSA和HSA的色氨酸残基进行特异性修饰后,Hg2+只引起NBS修饰的HSA的酪氨酸荧光轻微降低,但对NBS修饰的BSA的酪氨酸荧光几乎没有影响.远紫外和近紫外CD谱分析表明:Hg2+的结合要引起BSA,HSA以及NBS修饰的HSA二级结构的α螺旋减少,三级结构发生一定的改变.这些结果表明B 相似文献