扫描电化学显微镜及其界面电荷转移

扫描电化学显微镜（ScanningelectrochemicalmicroscopySECM）是一门电化学现场检测新技术，已经广泛应用于异相电子转移反应，吸、脱附过程，腐蚀过程、单细胞检测和液／液界面电子转移研究．本文就SECM的工作原理、操作模式和在界面分析中的应用做一简要综述．     

Species of Antarctoscyphus Peña Cantero,García Carrascosa and Vervoort, 1997 (Cnidaria: Hydrozoa: Symplectoscyphidae) collected by US Antarctic expeditions: biogeographic implications

Antarctoscyphus is one of the most characteristic genera of Antarctic benthic hydroids, with nine of the 10 known species considered to be endemic to the Antarctic; only Antarctoscyphus elongatus is also present in the sub-Antarctic region of Kerguelen. Accordingly, the genus was considered to have an Antarctic–Kerguelen distribution. Here we present the results of the study of the species of Antarctoscyphus collected from different Antarctic areas and from the Magellan region, during several expeditions under the United States Antarctic Research Program between 1958 and 1986. A scanning electron microscopy survey of all known species of the genus was carried out. Eight of the 10 known species of Antarctoscyphus were found in the collection, with A. spiralis and A. elongatus being the most frequently found species, whereas A. biformis, A. fragilis and A. gruzovi were found only once. The type material of A. biformis was reviewed and re-described. This study represents the second records for A. biformis and A. fragilis. The new records allow updating of the biogeographic knowledge on the distribution of several species: A. mawsoni, so far considered endemic to East Antarctica, and A. asymmetricus, considered endemic to West Antarctica, are here considered to have a Circum-Antarctic distribution. Additionally, A. fragilis, previously considered endemic to the Weddell Sea, is now considered to have a West Antarctic–Patagonian distribution, as it was recorded off the Pacific Magellan region. The records gathered here allow us to change the distribution pattern of the genus from Antarctic–Kerguelen to Pan-Antarctic. The study has allowed us to increase the known bathymetric range for some species, some reaching much deeper waters than previously known. Hence, A. fragilis, A. grandis and A. mawsoni, hitherto considered shelf species, are reported from bathyal bottoms of the continental slope. A general discussion on the bathymetric and geographic distribution of all known species is included.

www.zoobank.org/urn:lsid:zoobank.org:pub:1C7ED3F2-3FF1-4C5C-85BB-FAAF557AC2ED     

针对版权保护的图形图像数字水印算法

针对矢量图形数据和栅格图像数据的差异,围绕着数字水印算法的鲁棒性和透明性进行研究,提出了基于坐标漂移的图形数据水印算法和基于DCT的图像水印算法,并利用软件实现了数字水印的嵌入和提取.实验表明,这两种算法不仅满足数字水印透明性的要求,而且对于常规的数据攻击均具有很强的抵抗能力.     

P2O5对氟镓铟基玻璃析晶稳定性和结构的影响

以20GaF3-15InF3-20CdF2-15ZnF2-10SnF2-20PbF2(GICZSP)为基玻璃,用P2O5替代等摩尔含量CdF2,以改善玻璃的抗析晶能力.利用差示扫描量热分析、拉曼光谱和X射线衍射分析手段,表征不同含量P2O5对玻璃抗析晶性能及结构的影响.结果表明,P2O5的引入提高了玻璃的析晶稳定性.P2O5在玻璃中以不含P＝O双键的[PO(4-)4,Q0]四面体存在.随着P2O5量的增加,新出现了M[O,F]6八面体结构.     

校正几何失真和像素失真的印刷数字水印算法

针对印刷图像存在的几何失真和像素失真问题,提出一种数字水印算法.该算法采用Harris角点检测和Hausdorff距离来校正几何失真,采用非线性灰度变换来纠正像素失真.水印嵌入算法首先对图像进行一级离散小波变换后,再对低频子图进行奇异值分解;然后,在奇异值上嵌入水印序列,并在提取水印前校正失真.实验表明,该算法对打印扫...     

Real-time compensation of phase drift for phase-encoded quantum key distribution systems

Phase drift is an inherent problem in phase-encoded quantum key distribution(QKD) systems.The current active phase trackingand compensation solutions cannot satisfy the requirements of a system with nonlinearity in phase modulation.This paper presents a four-phase scanning method,which is based on the quantitative analysis of the quantum bit error rate(QBER) from phasedrift and the performance requirements of phase compensation.By obtaining the four interference fringes and adjusting the codingmatrix of the system,this method automatically calculates the accurate driving voltages for the phase modulator.The implementation and experimental tests show that the proposed method can compensate phase drift caused by environmental changes and thesystem’s nonlinearity,and is applicable to large-scale QKD networks.     

Synthesis and magnetic properties of Fe<Subscript>3</Subscript>O<Subscript>4</Subscript>/helical carbon nanofiber nanocomposites from the catalytic pyrolysis of ferrocene

High purity Fe3O4 /helical carbon nanofiber composites were obtained on a large scale by the catalytic pyrolysis of ferrocene in the presence of tin powder at 500°C over 12 h. The sizes of Fe 3 O 4 nanoparticles are 35–65 nm in size, and the diameters of the helical carbon nanofibers range from 40–70 nm. The shapes and compositions of the nanocomposites are simply controlled by adjusting the reaction temperatures. On the basis of the obtained experimental results the formation of the helical Fe3O4/carbon nanofiber composites was investigated and discussed. The magnetic hysteresis loop of the products shows ferromagnetic behavior with saturation magnetization (M s ), remanent magnetization (M r ) and coercivity (H c ) values of ca. 29.8 emu/g, 9.6 emu/g and 306.6 Oe, respectively.     

基于等角螺旋天线的GIS局部放电在线检测研究

对GIS局部放电的产生进行了分析,介绍了GIS局部放电的几种检测方法。着重论述了GIS特高频检测法和平面等角螺旋天线,探讨了如何使用特高频局部放电传感器进行现场测试。     

中国传统家具三维扫描和手工测绘的比较

提出了对中国传统家具进行测绘的基本原则、测绘内容。通过调研和实物试验,梳理了手工测绘的工具、方法和测绘流程,提出了三维立体扫描测绘的设备性能、方法和测绘过程,并对两种测绘方法进行了比较研究。使得家具的测绘、保护、生产设计的技术得到进一步改善,使传统家具文化与现代先进制造工艺得到更好的结合、传扬与发展。     

微波固相合成纳米LaB_6的组织结构及其透光特性

以La2O3和KBH4为原材料,用微波低温固相法合成LaB6纳米粉末。采用XRD衍射、Raman散射、扫描电镜和透射电镜对合成产物组织结构和分子振动进行表征。对添加LaB6纳米颗粒的聚乙烯醇缩丁醛(PVB)隔热透明涂层透光特性进行测试。研究结果表明:低温固相合成的LaB6结构与其他方法制备的LaB6结构相同,颗粒形状为类球形,其粒径在20～60 nm之间;含纳米LaB6颗粒的涂层对近红外辐射有明显的阻隔作用,在可见光区有良好的透过率;当添加纳米LaB6的质量分数为0.05%时,PVB涂层在可见过光区的透过率可达79%左右,在近红外光区的透过率只有46%。