Diamond synthesis from a system of chromium-carbide and Ni70Mn25Co5 alloy

In order to ascertain the mechanism of interaction between carbide and metallic catalyst and formation of diamond under high pressure and high temperature, and find a new method to synthesize diamond with special properties, it is necessary to investigate the reaction behavior of different carbides and metallic solvent_catalysts under high pressure and high temperature. A system of Cr-3C-2 powder and Ni 70Mn 25Co 5 alloy in weight ratio of 1∶6 was treated under 6 0 GPa and 1 500℃ for 20, 30 or 60 min respectively. X_ray diffraction of the samples indicated the Cr 3C 2 decomposed partially after high pressure and temperature treatment, and Cr 7C 3, Cr and diamond formed respectively. There was not any trace of graphite in the samples. The result suggested that the separated carbon atoms could form diamond directly without conversion process of graphite into diamond. The observation of SEI, WDX and EDX also showed that diamond crystals were synthesized in the system, which have perfect surfaces and shapes, with the average grain size of about 40 μm. The properties of the crystals are being investigated.     

Relationship between giant magnetoresistance of NiFe/Cu multilayers and their microstructures

The (111)-orientated NiFe/Cu multilayers were prepared by magnetron sputtering method. At room temperature, saturation magnetoresistances of NiFe/CU multilayers oscillate as a function of Cu spacer layer thickness. Two peak GMR values of 19.4%, 11.6% and 11.2%, 1% appear, respectively, at Cu sublayer thickness of t_Cu,= 1.0, 2.2 nm while the deposition pressures are 0.25 and 0.45 Pa. X-ray small-angle reflections and diffuse scattering at Cu K-edge (8.979 keV) by synchrotron radiation source were used to characterize the interfacial roughness. Diffraction anomalous fine-structure scattering (DAFS) was performed to investigate the local structure of NiFe and Cu sublayers. Results show that the deposition pressure has effect on interfacial roughness of the samples obviously, and the interfacial roughness also affects the GMR values of the samples strongly.     

支持CAD／CAPP／CAM集成和并行的制造特征

由于设计和制造过程的复杂性,目前还没有一种有效的方法能彻底解决产品设计、制造和生产管理等生命周期内各个阶段的信息集成问题．探讨了并行工程下的ＣＡＤ／ＣＡＰＰ／ＣＡＭ的集成框架,提出了支持ＣＡＤ／ＣＡＰＰ／ＣＡＭ集成和并行运行的制造特征,并在商品化ＣＡＤ／ＣＡＭ软件ＵＧⅡ上进行了开发工作．该系统已通过纺织行业箱体、柴油机行业的油泵以及机床厂的主轴箱等多种零件考核．     

1673K下BaO-BaF_2-Cr_2O_3渣系的热力学性质

１６７３Ｋ下,采用－ＭｏＣｒ＋Ｃｒ２Ｏ３ＺｒＯ２（ＭｇＯ）｛Ｃｕ＋Ｃｒ｝ａｌｏｙ＋（Ｃｒ２Ｏ３）ｓｌａｇＭｏ＋固体电解质电池测定了ＢａＯＢａＦ２Ｃｒ２Ｏ３渣系中Ｃｒ２Ｏ３的活度．研究结果表明,Ｃｒ２Ｏ３的活度随其浓度升高而升高,随ＸＢａＯ／ＸＢａＦ２升高而降低．根据实验及Ｘ射线衍射结果推测了该渣系的等温相图,并作出了该渣系中Ｃｒ２Ｏ３的等活度图．     

吸收比-系数倍率法及其应用——水杨酸钠、安替比林和咖啡因的同时测定

用吸收比－系数倍率法同时测定撒痛风注射液中水杨酸钠、安替比林和咖啡因三组分的含量。它们的回收率分别为１００．７％～１０２．１％、９５．９３％～１０４．５％和９７．５７％～１０１．７％。     

空化噪声特性实验研究

利用不同类型的轴对称头体和ＮＡＣＡ１６０１２翼型做了一系列空化噪声实验,得到轴对称头体在不同空化数及不同速度下的空化噪声谱及翼型在不同的攻角下的空化噪声谱．这一系列的噪声谱表明,各种轴对称头体的空化噪声总声级随空化数的减小而升高,但噪声谱形具有明显的相似形;翼型在片空化、泡空化和云雾空化状态下所辐射的噪声谱存在明显的差别．噪声总声级的变化较为复杂,由泡空化状态转换到片空化状态,空化数虽然减小,但总声级会突然降低．针对翼型在泡空化状态下所辐射噪声谱的特征,利用单空泡溃灭理论进行了尝试性的解释和说明．     

良好生产管理规范与全面质量管理及其在生物制品生产管理中的应用

从质量及生物制品质量的概念出发,阐述了良好生产管理规范（ＧＭＰ）管理模式和全面质量管理（ＴＱＣ）模式的基本内容及其在生物制品行业中的应用,认为ＴＱＣ是当今工业企业的现代化管理手段和方法,而ＧＭＰ是针对药品生产行业制定的一整套保证产品质量的基本要求．要想不断提高企业管理素质,改进产品质量,在生物制品企业中进行ＧＭＰ管理的同时,必须实行ＴＱＣ管理,ＴＱＣ所涉及的内容要比ＧＭＰ更广泛、更全面,而ＧＭＰ的实施又为ＴＱＣ的进行打下了良好的基础．     

莲子叶蛋白体的类型,来源与发育

莲子叶于发育的１０￣２８ｄ,以不同速率在叶肉细胞中大量积累贮存蛋白,并以不同方式组装许多形态各异、结构不同的蛋白体。按其来源与发育的特点可分４种类型：①粗面球状蛋白体;②光面球状蛋白体;③杯状蛋白体;④淀粉蛋白体。发育顺序是①,②类先形成,③,④类后发生;②类的发育贯穿整个贮存蛋白的积累期,比较了莲与其他植物蛋白体的异同。     

492QS射流燃烧室汽油机用活塞材质试验

讨论了用混合稀土对Ａｌ－Ｓｉ共晶合金的变质工艺,测定了合金的热抗拉强度、线膨胀系数和活塞的尺寸稳定性。结果表明：加入混合稀土１％后,ＺＬ１０８号合金铁热抗拉强度提高了２６％,线膨胀系数降低,活塞的尺寸稳定性增加。     

TiO2制备条件对光催化氧化活性的影响

半导体光催化剂,如ＴｉＯ２,在紫外光照射下,生成具有强氧化还原活性的电子和空穴,可使许多有机物降解为ＣＯ２和Ｈ２Ｏ,用于处理工业废水具有成本低,无二次污染等优点,是一种很有应用前景的废水催理方法［１,２］．制备高活性的ＴｉＯ２光催化剂是这种过程在处理...