慢回弹聚氨酯发泡体吸声性能研究

对不同泡孔大小、不同厚度慢回弹聚氨酯材料在不同频段下的吸声性能进行实验研究.研究表明,1 300 μm是材料泡孔大小对吸声性能影响的转折点.对于低频声波,泡孔直径为1 300 μm时,吸声性能最好;对中高频声波,吸声效果最差.材料厚度对吸声性能的影响,6 cm为最优值,此时材料的吸声效果最好;材料对不同频段声波的吸收效果也各不相同,频率为1 000 Hz声波的吸收效果最差,此频率是材料吸声性能的低谷.以上研究结果为工程使用提供了有价值的实验依据.     

放线菌生物活性物质的高通量筛选

 放线菌是产生生物活性物质最多的一类微生物.最近3年,我室从云南省采集土样,分离到3000多株放线菌、真菌,选择其中2600株,进行发酵,制备成提取物,利用自建的抗氧化、抑制乙酰胆碱酶、抑制一氧化氮合成酶、AGE等模型和高通量筛选系统进行了筛选,筛选到一些值得进一步研究的菌株.对高通量筛选的有关问题及初步筛选结果进行了讨论.     

试析民族地区大学英语教学中的“小题大做”

英语教学投入大,收益小,教师任重而道远。针对民族地区高校英语教学现状,结合多年教学经验,作者客观务实地提出教师应见微知著,从教学中的细小环节入手,做出提高大学英语教学质量的大文章来。     

Leaching Mechanism of Complicated Antimony-Lead Concentrate and Sulfur Formation in Slurry Electrolysis

Anodic reaction mechanism of complicated antimony-lead concentrate in slurry electrolysis was investigated by the anodic polarization curves determined under various conditions. The main reactions on the anode are the oxidations of FeCln^(2-n) . Though the oxidation of jamesonite particle on the anode can occur during the whole process, it is less. With the help of mineralogy studies and relevant tests, the leaching reaction mechanism of jameson[to and gudmundite during slurry electrolysis was ascertained. Because of the oxidation reaction of FeCl3 produced by antimony-lead concentrate itself, the non-oxidation complex acid dissolution of jameson[re, the oxidation complex acid dissolution of gudmundite, and the oxidation of air carried by stirring, the leaching ratio of antimony reaches about 35% when HCl-NH4Cl solution is used to leach antimony-lead concentrate directly. So when the theoretical electric quantity is given to oxidation of antimony in slurry electrolysis, all of antimony, lead and iron containing in antimony-lead concentrate, are leached. The formation of sulfur is through the directly redox reaction of Fe^3 and jameson[re. The S^2- in jamesonite is oxidized into S^0 , and forms the crystals of sulfur again on the spot. The redox reaction of Fe^3 and H2S formed by non-oxidative acid dissolution of jamesonite is less.     

冷气侧对流传热系数周期性波动对固体温度分布影响的一维分析

对边界对流传热系数正弦波动情况下一维固体非定常导热问题进行研究,考察无量纲化方程的解的特征,并以燃气轮机透平叶片冷却为背景,对方程进行数值求解,而后对方程中的主要无量纲量进行参数化分析.结果表明,影响固体内部无量纲温度分布的主要因素包括:无量纲位置X,无量纲时间Fo,以及固体两侧的毕渥数Bi_1和Bi_2;第三类边界条件的非线性会导致边界对流传热系数波动情况下壁面传热削弱,且削弱随着扰动频率的减小而加强;边界对流传热系数扰动的穿透深度主要受边界毕渥数变化频率f_(Bi_2)或波动角速度ω_(Fo)的影响.     

TTAC-HPMo/SiO_2催化剂的表征及其氧化脱硫性能分析

以十四烷基三甲基氯化铵(TTAC)为模板剂,正硅酸乙酯(TEOS)为硅源,采用溶胶-凝胶法制备TTAC-HPMo/SiO_2催化剂,利用FTIR、XRD、SEM和N_2吸附-脱附等技术对其进行表征,并分析催化剂制备条件和反应条件对模型油氧化脱硫性能的影响。结果表明,在m(HPMo)/m(SiO_2)=15%、焙烧温度为400℃条件下所制TTAC-HPMo/SiO_2催化剂,其孔隙结构发达、氧化脱硫性能最佳;对于10mL以二苯并噻吩(DBT)为目标含硫化合物的模型油(硫含量为400μg/g),当m(TTAC-HPMo/SiO_2)/m(模型油)=0.43%、V(H_2O_2)/V(模型油)=0.2%、反应温度为60℃、反应时间为14min时,所制TTAC-HPMo/SiO_2催化剂对模型油中DBT的脱除率达到100%。     

Effects of Cr and Mo elements on the microstructures and compressive properties of the in situ (TiC_xN_y–TiB_2)/Ni cermets

In-situ(TiC_xN_y–TiB_2)/Ni cermets with 70 wt%TiC_xN_y–TiB_2 were successfully fabricated by combustion synthesis and hot pressing sintering in Ni-Ti-B_4C-BN powder systems.The microstructures,density,compressive properties,and hardness of the TiC_xN_y–TiB_2/Ni cermets with the addition of 0–8 wt%Cr/Mo to the Ni-Ti-B_4C-BN powder systems were compared and analysed.The results showed that the ceramic particles distributed uniformly in the cermets,and the size of the ceramic particles reduced with the Cr/Mo addition.Both Cr and Mo addition can improve the hardness,compressive properties,and fracture strains of the cermets.The hardness,compressive strength,and fracture strain of the(TiC_xN_y–TiB_2)/(Ni+Cr)cermets increased from 1561 HV,2.94 GPa,and 2.9%to 1864 HV,3.65 GPa,and 3.4%,respectively when the Cr content increased to 5 wt%.The hardness and compressive strength of the(TiC_xN_y–TiB_2)/(Ni+Mo)cermets increased from 1561 HV and 2.94 GPa to 1902 HV and 3.43 GPa,respectively when the Mo content increased to 8 wt%.The cermets with Cr had better compressive properties than the cermets with Mo.     

介质流向对截止阀流场和流阻特性的影响

为探索介质流向对截止阀内部流场和流阻特性的影响,应用SOLIDWORKS软件建立截止阀的三维模型。使用Fluent软件中的有限元法和标准k-ε湍流模型,在不同开度的情况下,采用数值模拟分析的方法,研究不同介质流向下截止阀的流场和流阻特性,分析阀体内部的速度和压力分布规律。结果表明:在两种不同的流向下,阀门的流通能力相差较小;在小开度时,介质高进低出时能够减小阀门的压力损失,在流通高压介质的情况下,高进低出的流向能够极大的减小阀门的关闭力。流场的分析为截止阀的结构设计和优化提供参考。     

基于跳跃滤波和时变参数估计的中国股市微观结构研究

为了更为有效地探究微观市场结构对股票价格的影响,本文在状态空间模型框架下,同时将交易方向、带方向的交易量、交易间隔、微观噪声以及跳跃因素引入状态方程和观测方程中,建立全面的市场微观结构模型,以反映各变量对交易价格序列产生的暂时性和永久性影响.然后,在采用基于粒子滤波的非参数离群点检测方法检测跳跃并对跳跃进行滤波的基础上,运用贝叶斯最小二乘方法对微观结构模型系数、波动率以及状态变量进行实时更新和估计,在此基础上分析跳跃日度分布、日内分布、个股跳跃和共同跳跃特征,并同时判断不同交易方向、交易量的订单对价格产生的影响.最后选取2015年股灾期间、沪市股票的逐笔数据作为研究样本进行实证研究.实证结果显示:我国股票高频时间序列跳跃和共同跳跃均存在日内季节性,且跳跃频率和大小与市场信息密切相关;买卖订单对交易价格及股票价值的影响并不是完全对称的,交易价格对于微观结构的敏感度、微观结构噪声也随市场波动而发生变化,熊市中都相对更高;考虑跳跃滤波并对参数进行实时估计可以提高价格对于交易的敏感度,能更好地捕捉市场微观结构在价格发现中的作用.