Effect of minor Sc on the microstructure and mechanical properties of AZ91 Magnesium Alloy

The as-cast and heat-treated microstructures and mechanical properties of the AZ91 magnesium alloys with and without minor Sc addition were investigated and compared in this paper. The results indicated that adding0.15–0.45 wt% Sc to the as-cast AZ91 alloy not only could modify and refine the Mg_(17)Al_(12) phase but also suppress the formation of the Mg_(17)Al_(12) phase. At the same time, the grains of the Sc-containing as-cast AZ91 alloys were also effectively refined. As a result, the mechanical properties at room temperature(RT) for the Sccontaining as-cast AZ91 alloys were effectively improved. In addition, adding 0.15–0.45 wt%Sc to the AZ91 alloy promoted the formation of the continuous precipitates(CP) during the aging treatment in spite of that the formation of the discontinuous precipitates(DP) was simultaneously suppressed. Accordingly, the Sc-containing as-aged AZ91 alloys obtained the relatively higher mechanical properties at RT than the as-aged AZ91 alloy.     

高校绩效审计的开展及其必然性分析

随着以现代科学技术为核心,建立在知识和信息的生产、分配和使用上的新经济时代的到来,我国高校经费投入开始持续增加,办学规模不断扩大.但由于我国大部分高校教学基础设施薄弱,教育资金远远不能满足建设和发展的需求,教育经费使用效益不高的问题持续发酵,很大程度上制约了我国高校的教学质量.如何理解新经济时代对高校审计的影响已经成为开展高校绩效审计面临的重要难题.论述了新经济时代的特征、对高校审计的影响,简单概述了绩效审计的发展历程以及国内外高校绩效审计发展现状,从而进一步阐明新经济时代开展高校绩效审计的必要性.     

基于RSM和FEM的辊锻件长度控制技术

以某钩尾框精密辊锻工艺为研究对象,首次应用响应面法(RSM)和有限元数值模拟法(FEM)对精密辊锻件的长度控制问题进行了研究.首先以满足辊锻件长度和降低轧辊最大扭矩为目标,采用FORGE3有限元软件建立了RSM与FEM相结合的二阶分析模型,研究了轧辊间隙、摩擦因子、轧辊转速和坯料温度对辊锻件的长度和轧辊最大扭矩的显著性和影响规律;其次采用优化后的工艺参数对该辊锻工艺进行了再模拟,提出了辊锻件长度的调试原则,利用该原则和点的反追踪技术对辊锻模具进行了再设计,同时分析了设计、模拟和生产辊锻件的长度和辊锻过程的功率耗散和分布.研究结果表明:应用RSM和FEM可准确有效地掌握精密辊锻件的长度控制技术.     

融合词法句法分析联合模型的树到串EBMT方法

针对传统的基于实例的机器翻译(EBMT)方法中系统构筑复杂度和成本较高的问题,提出一种基于依存树到串的汉英实例机器翻译方法。与传统方法相比,该方法只需进行源语言端的句法结构分析,可以大大降低构筑系统的复杂度,有效降低成本。为了提高翻译精度,引入中文分词、词性标注和依存句法分析联合模型,可以减少汉英EBMT中源语言端基础任务中的错误传递,提高提取层次间特征的准确性。在此基础上,结合依存结构的特征和中英语料的特性,对依存树到串模型进行规则抽取以及泛化处理。实验结果表明,相对于基线系统,该方法可以提高实例对抽取质量,改善泛化规则和译文质量,提高系统性能。     

Effect of Ce addition on hot tearing behavior of AZ91 alloy

A small amount of cerium (below 1.0 wt%) addition to AZ91 alloy have been investigated on the hot tearing susceptibility (HTS) at a cooling rate of 1.5Ks^?1. The HTS increased to a maximum value with a cerium addition of 0.6 wt% and then decreased to a stable status as cerium was gradually added. Due to high chemical activity, cerium into the melts can react with aluminum to form an Al₁₁Ce₃ intermetallic compound. X–ray diffraction results also confirmed the existence of Al₁₁Ce₃. The Al₁₁Ce₃ increased with the presence of the needle-like and block morphology. As cerium levels increased, the amount of Mg₁₇Al₁₂ decreased. The variations between Mg₁₇Al₁₂ and Al₁₁Ce₃ resulted in a similar normal distribution of the HTS in AZ91 alloy. The findings were further verified through the microstructure evolution and the surface morphology of fracture.     

基于广义出行成本的出行方案优化

为了使出行成本更加符合出行者的认知规律,运用结构方程建模方法模拟出行成本,个体特征及出行决策之间的影响关系.引入敏感系数调整服务属性在出行成本中的贡献率,利用出行意愿调查数据对敏感系数进行标定.考虑出行者对抵达时刻的选择偏好,假设行程时间服从正态分布条件下,对最佳出发时刻及期望出行成本进行寻优求解,结果表明它取决于期望到达时刻,行程时间的期望值及方差,出行者对早到损失及晚到延误损失时间成本的相对大小.研究成果可为制定个性化及最优化出行决策方案提供依据.     

基于树状分子及炭黑复合纳米材料修饰电极的Cr(VI)电化学检测

用树状分子及炭黑纳米复合材料修饰玻碳电极,并对六价铬Cr(VI)进行电化学测定.采用X射线光电子能谱(XPS)、循环伏安法(CV)、交流阻抗法(EIS)、方波溶出伏安法(SWSV)等方法对修饰电极进行了表征.研究发现多种其他离子如Ni~(2+)、Co~(2+)、Pb~(2+)、Cu~(2+)、Cd~(2+)、NO_3~-、SO_4~(2-)、Cl~-等对六价铬离子的测定没有明显干扰,且Cr(VI)的还原峰电流与Cr(VI)的物质的量浓度在4~60 nmol/L和0.06~500μmol/L范围内呈线性关系,检测限达1 nmol/L.该法具有简便快速,选择性好,线性范围宽,灵敏度高等优点.     

Cobalt doped titanate nanotubes: Synthesis and properties

Cobalt oxide doped titanate nanotubes are synthesized with a simple hydrothermal treatment of mixed Co_3O_4 and TiO_2 powders. The formed tubular nanostructure, chemical composition,and the elemental distribution are analyzed using TEM, BET, FTIR, XRD, and XPS. The electrocatalytic activity towards oxygen evolution reactions and photodegradation against Rhodamine B are investigated. It has been found out that the oxygen evolutions starts at 0.8 V and reaches 0.98 mA ·cm~(–1) at 1.4 V vs. SCE. For photodegradation of Rhodamine B, the concentration decreased to 24% after 1 h irradiation using the sample with a mass percentage of 5% cobalt. The results demonstrate that the cobalt oxide doped titanate nanotubes are good candidates as electrocatalysts and photocatalytic materials.