电弧填丝增材制造高强度低合金钢的组织和力学性能

A high-building multi-directional pipe joint (HBMDPJ) was fabricated by wire and arc additive manufacturing using high-strength low-alloy (HSLA) steel. The microstructure characteristics and transformation were observed and analyzed. The results show that the forming part includes four regions. The solidification zone solidifies as typical columnar crystals from a molten pool. The complete austenitizing zone forms from the solidification zone heated to a temperature greater than 1100°C, and the typical columnar crystals in this zone are difficult to observe. The partial austenitizing zone forms from the completely austenite zone heated between Ac1 (austenite transition temperature) and 1100°C, which is mainly equiaxed grains. After several thermal cycles, the partial austenitizing zone transforms to the tempering zone, which consistes of fully equiaxed grains. From the solidification zone to the tempering zone, the average grain size decreases from 75 to 20 μm. The mechanical properties of HBMDPJ satisfies the requirement for the intended application.     

基于EBSD数据，采用考虑各向异性效应的改进蒙特卡罗模型对冷轧超薄晶粒取向硅钢的再结晶过程进行了模拟

A Monte Carlo Potts model was developed to simulate the recrystallization process of a cold-rolled ultra-thin grain-oriented silicon steel. The orientation and image quality data from electron backscatter diffraction measurements were used as input information for simulation. Three types of nucleation mechanisms, namely, random nucleation, high-stored-energy site nucleation (HSEN), and high-angle boundary nucleation (HABN), were considered for simulation. In particular, the nucleation and growth behaviors of Goss-oriented ({011}<100>) grains were investigated. Results showed that Goss grains had a nucleation advantage in HSEN and HABN. The amount of Goss grains was the highest according to HABN, and it matched the experimental measurement. However, Goss grains lacked a size advantage across all mechanisms during the recrystallization process.     

烧结温度对纳米石墨烯增强ZA27基复合材料孔隙比和力学性能的影响

Nano graphene platelet (Gr) reinforced nano composites with a zinc–aluminum alloy (ZA27) matrix were produced by powder metallurgy at four different mass ratios (0.5wt%, 1.0wt%, 2.0wt% and 4.0wt%) and three different sintering temperatures (425, 450, and 475°C). In order to investigate the effect of sintering temperatures and nano graphene reinforcement materials on the composite structure, the microstructures of the composite samples were investigated and their densities were determined with a scanning electron microscope. Hardness, transverse rupture, and abrasion wear tests were performed to determine the mechanical properties. According to the test results, the porosity increased and the mechanical strength of the nano composites decreased as the amount of nano graphene reinforcement in ZA27 increased. However, when the composites produced in different reinforcement ratios were evaluated, the increase in sintering temperature increased the mechanical structure by positively affecting the composite structure.     

煤田火灾的形成机理及其探测和控制技术

Coalfield fires are considered a global crisis that contributes significantly to environmental destruction and loss of coal resources and poses a serious threat to human safety and health. In this paper, research related to the initiation, development, and evolution of coalfield fires is reviewed. The existing detection and control techniques of coalfield fires are also reviewed. Traditional firefighting is associated with waste of resources, potential risks of recrudescence, potential safety hazards, extensive and expensive engineering works, and power shortages. Recently, coalfield fires have been recognized as having significant potential for energy conservation and heat energy recovery. Thermoelectric power generation is regarded as a suitable technology for the utilization of heat from coalfield fires. The extraction of heat from coalfield fires can also control coalfield fires and prevent reignition leading to combustion. Technologies for absorbing heat from burning coal and overlying rocks are also analyzed. In addition, the control mode of “three-region linkage” is proposed to improve firefighting efficiency. Integrating heat energy recovery with firefighting is an innovative method to control coalfield fires.     

焊接速度对自适应双轴肩搅拌摩擦焊接Al–Mg合金接头微观组织和机械性能的影响

The butt welds of 4-mm thick 5A06 aluminum alloy plates were produced by adjustable-gap bobbin-tool friction stir travel with travel speeds of 200, 300, and 400 mm/min in this study. The microstructure was studied using optical microscopy and electron backscatter diffraction (EBSD). Tensile tests and microhardness measurements were performed to identify the effect of the travel speed on the joint mechanical properties. Sound joints were obtained at 200 mm/min while voids were present at different positions of the joints as the travel speed increased. The EBSD results show that the grain size, high angle grain boundaries, and density of geometrically necessary dislocations in different regions of the joint vary depending on the recovery and recrystallization behavior. Specific attention was given to the relationship between the local microstructure and mechanical properties. Microhardness measurements show that the average hardness of the stir zone (SZ) was greater than that of the base material, which was only affected slightly by the travel speed. The tensile strength of the joint decreased with increasing travel speed and the maximal strength efficiency reached 99%.     

增材制造镍基高温合金IN718的热处理优化

Additive manufacturing (AM) of Ni-base superalloy components can lead to a significant reduction of weight in aerospace applications. AM of IN718 by selective laser melting results in a very fine dendritic microstructure with a high dislocation density due to the fast solidification process. The complex phase composition of this alloy, with three different types of precipitates and high residual stresses, necessitates adjustment of the conventional heat treatment for AM parts. To find an optimized heat treatment, the microstructures and mechanical properties of differently solution heat-treated samples were investigated by transmission and scanning electron microscopy, including electron backscatter diffraction, and compression tests. After a solution heat treatment (SHT), the Nb-rich Laves phase dissolves and the dislocation density is reduced, which eliminates the dendritic substructure. SHT at 930 or 954°C leads to the precipitation of the δ-phase, which reduces the volume fraction of the strengthening γ′- and γ′′-phases formed during the subsequent two stage aging treatment. With a higher SHT temperature of 1000°C, where no δ-phase is precipitated, higher γ′ and γ′′ volume fractions are achieved, which results in the optimum strength of all of the solution heat treated conditions.     

搅拌摩擦法和搅拌摩擦振动法制备镁表面纳米复合材料的对比研究

Friction stir processing (FSP) can be used to improve surface composites. In this study, a modified method of FSP called friction stir vibration processing (FSVP) was applied to develop a surface composite on AZ91 magnesium alloy. In this technique, the workpiece is vibrated normal to the processing direction. The results illustrated that compared with the FSP method, the FSVP caused a better homogeneous distribution of SiC particles in the microstructure. The results also showed that matrix grains of friction stir vibration processed (FSV-processed) samples ((26.43 ± 2.00) μm) were finer than those of friction stir processed (FS-processed) specimens ((39.43 ± 2.00) μm). The results indicated that the ultimate tensile strength (UTS) of FSV-processed specimens (361.82 MPa) was higher than that of FS-processed specimens (324.97 MPa). The higher plastic strain in the material during FSVP, due to workpiece vibration, resulted in higher dynamic recrystallization, and consequently, finer grains were developed. The elongation and formability index of the FSV-processed specimen (16.88% and 6107.52 MPa·%, respectively) were higher than those of the FS-processed sample (15.24% and 4952.54 MPa·%, respectively). Moreover, the effects of FSVP were also found to intensify as the vibration frequency increased.     

结晶器内电磁搅拌对结晶器表面负偏析影响的模型预测

Aiming at the problem of negative segregation under a bloom surface, a coupling macrosegregation model considering electromagnetic field, flow, heat, and solute transport was established based on the volume average method to study the effect of in-mold electromagnetic stirring (M-EMS) on the negative segregation under the bloom surface. In the model, the influence of dendrite structure on the flow and solute transport was described by the change of permeability. The model was validated by the magnetic induction intensity of M-EMS and carbon segregation experiment. The results show that the solute C in the solidified shell in the turbulent zone of the bloom undergoes two negative segregations, whereby the first is caused by nozzle jet, and the second by the M-EMS. The severities of the negative segregation caused by M-EMS at different currents and frequencies are also different, and the larger the current is, or the smaller the frequency is, the more serious will be the negative segregation. With the M-EMS, the solute C distribution in the liquid phase of the bloom is more uniform, but the mass fraction of C in the liquid phase is higher than that without M-EMS.     

通过高温预处理高磷鲕状赤铁矿实现铁富集和脱磷

The efficient development and utilization of high-phosphorus oolitic hematite is of great strategic significance for the sustainable supply of iron-ore resources in China. In this paper, the mechanism of high-temperature pretreatment for enhancing the effect of iron enrichment and dephosphorization in the magnetization roasting–leaching process was studied by X-ray diffraction (XRD), vibration sample magnetometer (VSM), scanning electron microscopy and energy dispersive spectrometry (SEM–EDS). Compared with the process without high-temperature pretreatment, the iron grade of the magnetic separation concentrate after high-temperature pretreatment had increased by 0.98%, iron recovery rate had increased by 1.33%, and the phosphorus content in the leached residue had decreased by 0.12%. High-temperature pretreatment resulted in the dehydration and decomposition of hydroxyapatite, the dehydration of limonite and the thermal decomposition of siderite, which can produce pores and cracks and weaken the compactness of the ore, improve the magnetization characteristics of roasted ore, and strengthen the iron enrichment and dephosphorization during the magnetization roasting and leaching process.     

初始ECAP道次对5083铝合金晶织构和残余应力的影响

To produce a highly refined microstructure, several metals or alloys have been processed via equal-channel angular pressing (ECAP). In this work, the mechanical and microstructural changes of the 5083 aluminum alloy in H11 condition after processed by two ECAP passes were investigated. An ECAP H13 steel die with an inner angle (α) of 120° and outer curvature (β) of 20° was used. The microstructural changes were associated with the loss of texture symmetry. The morphologies of the Mg₂Si and α-Al(Mn,Fe)Si precipitates for the sample at the initial condition were similar to those subjected to two ECAP passes. The peak broadening measured by X-ray diffraction revealed an increment of both grain refinement and microstrain. After the second extrusion pass, the hardness increased by 62% compared with the initial condition. Moreover, the heterogeneous hardness behavior was compatible with a highly localized dislocation density. After two ECAP passes, shear parallel bands were observed to be at nearly 45° to the extrusion direction. The evaluation of first-order residual stress as a function of the depth of the analyzed sample displayed compressive or tensile values, depending on the measured face. With the plastic deformation applied, the first and second-order residual stresses exhibited significant increment. Williamson-Hall plots showed positive slopes, indicating an increment in the microstrain.     

Characterization of Ordovician carbonate reservoirs, southeastern Saskatchewan, Canada

The discovery of the prolific Ordovician Red River reservoirs in 1995 in southeastern Saskatchewan was the catalyst for extensive exploration activity which resulted in the discovery of more than 15 new Red River pools. The best yields of Red River production to date have been from dolomite reservoirs. Understanding the processes of dolomitization is, therefore, crucial for the prediction of the connectivity, spatial distribution and heterogeneity of dolomite reservoirs.The Red River reservoirs in the Midale area consist of 3～4 thin dolomitized zones, with a total thickness of about 20 m, which occur at the top of the Yeoman Formation. Two types of replacement dolomite were recognized in the Red River reservoir: dolomitized burrow infills and dolomitized host matrix. The spatial distribution of dolomite suggests that burrowing organisms played an important role in facilitating the fluid flow in the backfilled sediments. This resulted in penecontemporaneous dolomitization of burrow infills by normal seawater. The dolomite in the host matrix is interpreted as having occurred at shallow burial by evaporitic seawater during precipitation of Lake Almar anhydrite that immediately overlies the Yeoman Formation. However, the low δ18O values of dolomited burrow infills (-5.9‰～ -7.8‰, PDB) and matrix dolomites (-6.6‰～ -8.1‰, avg. -7.4‰ PDB) compared to the estimated values for the late Ordovician marine dolomite could be attributed to modification and alteration of dolomite at higher temperatures during deeper burial, which could also be responsible for its 87Sr/86Sr ratios (0.7084～0.7088) that are higher than suggested for the late Ordovician seawaters (0.7078～0.7080). The trace amounts of saddle dolomite cement in the Red River carbonates are probably related to "cannibalization" of earlier replacement dolomite during the chemical compaction.     

A computer generator for randomly layered structures

AcomputergeneratorforrandomlylayeredstructuresYUJia shun1,2,HEZhen hua2(1.TheInstituteofGeologicalandNuclearSciences,NewZealand;2.StateKeyLaboratoryofOilandGasReservoirGeologyandExploitation,ChengduUniversityofTechnology,China)Abstract:Analgorithmisintrod…     

海南岛地体及其毗邻陆缘晚中生代—新生代古地磁研究和构造演化

本文叙述了对海南岛及其毗邻大陆边缘白垩纪到第四纪地层岩石进行古地磁研究的全部工作过程。通过分析岩石中剩余磁矢量的磁偏角及磁倾角的变化,提出海南岛白垩纪以来经历的构造演化模式如下:早期伴随顺时针旋转而向南迁移,后期伴随逆时针转动并向北运移。联系该地区及邻区的地质、地球物理资料,对海南岛上述的构造地体运动提出以下认识:北部湾内早期有一拉张作用,主要是该作用使湾内地壳显著伸长减薄,形成北部湾盆地。从而导致了海南岛的早期构造运动,而海南岛后期的构造运动则主要是受南海海底扩张的影响。海南地体运动规律的阐明对于了解北部湾油气盆地的形成演化有重要的理论和实际意义。     

Exciton Seebeck in Molecular Systems

Various applications relevant to the exciton dynamics,such as the organic solar cell,the large-area organic light-emitting diodes and the thermoelectricity,are operating under temperature gradient.The potential abnormal behavior of the exicton dynamics driven by the temperature difference may affect the efficiency and performance of the corresponding devices.In the above situations,the exciton dynamics under temperature difference is mixed with     

Achieving Unusual States of Matter Under High Pressure

The elongation method,originally proposed by Imamura was further developed for many years in our group.As a method towards O(N)with high efficiency and high accuracy for any dimensional systems.This treatment designed for one-dimensional(ID)polymers is now available for three-dimensional(3D)systems,but geometry optimization is now possible only for 1D-systems.As an approach toward post-Hartree-Fock,it was also extended to     

《Chinese Science Bulletin》SUBJECT INDEX TO VOLUME 59(2014)

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An on-line scaling method for improving scalability of a database cluster

The explosive growth of the Internet and database applications has driven database to be more scalable and available, and able to support on-line scaling without interrupting service. To support more client's queries without downtime and degrading the response time, more nodes have to be scaled up while the database is running. This paper presents the overview of scalable and available database that satisfies the above characteristics. And we propose a novel on-line scaling method. Our method improves the existing on-line scaling method for fast response time and higher throughputs. Our proposed method reduces unnecessary network use, i.e. , we decrease the number of data copy by reusing the backup data. Also, our on-line scaling operation can be processed parallel by selecting adequate nodes as new node. Our performance study shows that our method results in significant reduction in data copy time.     

An improved R-tree based on childnode''s probability

R-Tree is a good structure for spatial searching. But in this indexing structure,either the sequence of nodes in the same level or sequence of traveling these nodes when queries are made is random. Since the possibility that the object appears in different MBR which have the same parents node is different, if we make the subnode who has the most possibility be traveled first, the time cost will be decreased in most of the cases. In some case, the possibility of a point belong to a rectangle will shows direct proportion with the size of the rectangle. But this conclusion is based on an assumption that the objects are symmetrically distributing in the area and this assumption is not always coming into existence. Now we found a more direct parameter to scale the possibility and made a little change on the structure of R-tree, to increase the possibility of founding the satisfying answer in the front sub trees. We names this structure probability based arranged R-tree (PBAR-tree).     

Integrating GIS Web services based on mediating architecture

The geographic information service is enabled by the advancements in general Web service technology and the focused efforts of the OGC in defining XML-based Web GIS service. Based on these models, this paper addresses the issue of services chaining,the process of combining or pipelining results from several interoperable GIS Web Services to create a customized solution. This paper presents a mediated chaining architecture in which a specific service takes responsibility for performing the process that describes a service chain. We designed the Spatial Information Process Language (SIPL) for dynamic modeling and describing the service chain, also a prototype of the Spatial Information Process Execution Engine (SIPEE) is implemented for executing processes written in SIPL. Discussion of measures to improve the functionality and performance of such system will be included.     

Tracking data management using topology of moving object database system for moving object constrained trajectory in LBS application

Advances in wireless technologies and positioning technologies and spread of wireless devices, an interest in LBS (Location Based Service) is arising. To provide location based service, tracking data should have been stored in moving object database management system (called MODBMS) with proper policies and managed efficiently. So the methods which acquire the location information at regular time intervals then, store and manage have been studied. In this paper, we suggest tracking data management techniques using topology that is corresponding to the moving path of moving object. In our techniques, we update the MODBMS when moving object arrived at a street intersection or a curved road which is represented as the node in topology and predict the location at past and future with attribute of topology and linear function. In this technique, location data that are corresponding to the node in topology are stored, thus reduce the number of update and amount of data. Also in case predicting the location,because topology are used as well as existing location information, accuracy for prediction is increased than applying linear function or spline function.