Zircon U-Pb SHRIMP dating for the volcanic rocks of the Xiong’er Group: Constraints on the initial formation age of the cover of the North China Craton

The volcanic rocks of the Xiong‘er Group occur widely in the southern part of the North China Craton, which mark the beginning of the cover in the southern part of the North China Craton. The age of the volcanic rocks is thus crucial to understand the tectonic regime and evolutionary history of the North China Craton in the Proterozoic age. Zircons from five volcanic rocks and intrusions were dated by U-Pb SHRIMP method. The results indicate that the Xiong‘er Group formed in 1.80--1.75 Ga of Paleo-Proterozoic. Since the Xiong‘er Group formed earlier than the Changcheng System, the earliest rocks in the Changcheng System is therefore assumed to be formed in 1.75 Ga. A thermal-tectonic event of ca. 1.84 Ga is indicated by new zircon U-Pb SHRIMP ages in the southern part of the North China Craton. The volcanic rocks of the Xiong‘er Group thus represent the initial magmatism of the Paleo-Proterozoic breakup of the North China Craton. Numerous inherited zircons in the volcanic rocks mainly formed in ～2.20 Ga, indicating that the source magma of the volcanic rocks may be derived from the ～2.20 Ga crust, or from a mantle magma with significant contamination of the ～2.20 Ga crust.     

U–Pb ages and Hf isotopes for detrital zircons from quartzite in the Paleoproterozoic Songshan Group on the southwestern margin of the North China Craton

In situ U-Pb dating and Lu-Hf isotopic analysis were carried out for detrital zircons from quartzite in the Paleoproterozoic Songshan Group on the southern margin of the North China Craton (NCC). The re- sults provide further constraints on the crustal formation and evolution history of NCC. Four 207Pb/206Pb age populations were obtained from 99 analyses, with clusters at ~3.40 Ga, 2.77―2.80 Ga, ~2.50 Ga and 2.34 Ga, respectively. The 3.40 Ga old zircons have similar Hf isotopic compositions to those from Ar- chean rocks in the Jidong and Anshan areas of NCC. However, crustal remnants older than 3.6 Ga have been identified in the southern margin of NCC, the South China Craton, the northwestern part of the Qinling Orogen and its adjacent area. Thus, it is not easy to trace the source rock from which the 3.40 Ga detrital zircons were derived. It can be inferred that the crustal remnants older than 3.40 Ga might have been widely distributed in the North China Craton. The 2.77―2.80 Ga zircons make up a relatively small proportion and have the highest εHf (t) values (up to 6.1±1.6), consistent with the Hf isotopic composition of the depleted mantle at 2.83 Ga. Their single-stage Hf model age of 2.83 Ga is close to their crystallized age, suggesting that their source rocks were extracted from the contemporaneous depleted mantle. The ~2.50 Ga zircon grains constitute about 85% of the total grain population and their Hf isotopic compositions indicate major growth of juvenile crust at ~2.50 Ga but minor reworking of ancient crust. The youngest zircon dated in this study gave an U-Pb age of 2337±23 Ma, which can be considered the maximum depositional age of the formation of the Songshan Group.     

SHRIMP U-Pb geochronology of the zircons from the Precambrian basement of the Qilian Block and its geological significances

Origin and tectonic evolution of the Qilian Precambrian basement on NW China were investigated using zircon U-Pb ages with collaborating stratigraphic and paleontological evidence. Zircon grains were separated from two schists, two granitic gneisses and one mylonized gneiss and dated with SHRIMP. Seventy percent of sixty-one detrital zircon ages from two schists ranges from 0.88 Ga to 3.09 Ga, mostly within 1.0 Ga to 1.8 Ga with a peak at 1.6 Ga to 1.8 Ga, and twenty percent varies from 2.0 Ga to 2.5 Ga. A few falls in the Archean and Neoproterozoic periods. The two granitic gneisses were dated 930±8 Ma and 918±14 Ma, whereas the mylonized granitic gneiss was dated 790±12 Ma. These ages represent two periods of magmatisms, which can be correlated with the early and late stages of magmatisms associated with the Jinningian movement on the Yangtze Blocks. The results from this and previous studies indicate that the ages of the Precambrian detrital zircons from the Qilian Block are widely distributed in the Proterozoic era, distinct from the North China Block which was stable in the Neo-Mesoproterozoic era. By contrast, the age histograms of the detrital zircons from the Qilian Block is similar to those from Precambrian basement of the Yangtze Craton. Therefore, it is suggested that the Qilian Block had a strong affinity toward the Yangtze Craton and might belong to the supercontinent Gondwana in the Neoproterozoic time. This inference is supported by Nd model age (TDM), stratigraphic, and paleontological evidence. It is further considered that the Qilian Block was rifted from the supercontinent Gondwana during late Sinian to form an isolated continent in the Proto-Tethyan Ocean, moving towards the Alaxa Block in the North China Craton. The part of Proto-Tethyan Ocean between the Qilian and Alaxa Blocks should correspond to the so-called Paleo-Qilian Ocean. Following the closure of the Paleo-Qilian Ocean in the early Paleozoic, the Qilian Block collided with the Alaxa Block to form the North Qilian Orogenic Belt. Based on this tectonic explanation, the North Qilian ophiolites should represent parts of lithosphere from the Proto-Tethyan Ocean. Lithological and geochronological evidence also indicates that the Qilian Block underwent continental reactivation possibly induced by the deep northward subduction of the North Qaidam Block in early Paleozoic time.     

U-Pb ages and Hf isotopes for detrital zircons from quartzite in the Paleoproterozoic Songshan Group on the southwestern margin of the North China Craton

In situ U-Pb dating and Lu-Hf isotopic analysis were carried out for detrital zircons from quartzite in the Paleoproterozoic Songshan Group on the southern margin of the North China Craton （NCC）. The results provide further constraints on the crustal formation and evolution history of NCC. Four ^207Pb/^206Pb age populations were obtained from 99 analyses, with clusters at -3.40 Ga, 2.77-2.80 Ga, -2.50 Ga and 2.34 Ga, respectively. The 3.40 Ga old zircons have similar Hf isotopic compositions to those from Archean rocks in the Jidong and Anshan areas of NCC. However, crustal remnants older than 3.6 Ga have been identified in the southern margin of NCC, the South China Craton, the northwestern part of the Qinling Orogen and its adjacent area. Thus, it is not easy to trace the source rock from which the 3.40 Ge detrital zircons were derived. It can be inferred that the crustal remnants older than 3.40 Ga might have been widely distributed in the North China Craton. The 2.77-2.80 Ga zircons make up a relatively small proportion and have the highest εHf（t） values （up to 6.1±1.6）, consistent with the Hf isotopic composition of the depleted mantle at 2.83 Ga. Their single-stage Hf model age of 2.83 Ga is close to their crystallized age, suggesting that their source rocks were extracted from the contemporaneous depleted mantle. The -2.50 Ga zircon grains constitute about 85% of the total grain population and their Hf isotopic compositions indicate major growth of juvenile crust at -2.50 Ga but minor reworking of ancient crust. The youngest zircon dated in this study gave an U-Pb age of 2337±2.3 Ma, which can be considered the maximum depositional age of the formation of the Songshan Group.     

SHRIMP U-Pb geochronology of the detrital zircons from the Longshoushan Group and its tectonic significance

Sixty-two geologically meaningful U-Pb dates were obtained by using SHRIMP technique for the detrital zircons in three metasedimentary rocks from stratigraphically uppermost parts of the Longshoushan Group in the present study. Eighty percents of these dates range from 1.7 Ga to 2.2 Ga with a peak at 1.8-2.0 Ga and twenty percents from 2.3 Ga to 2.7 Ga. The youngest detrital zircon is dated at 1724±19 Ma which is interpreted as the maximum depositional age of the metasedimentary rocks. Therefore, the age for the diagenesis and lithification of the original sedimentary rocks of the Longshoushan Group before the metamorphism must be younger than 1724±19 Ma. Comparison of the age histograms of these detrital zircons with the ages of the igneous rocks on the surrounding older massifs suggests that the sediments of the Longshoushan Group were most likely derived from the Alaxa Block and Tarim Craton. This implies that the affinity between Alaxa Block and Tarim Craton was strong and that they might have been a unified craton during middle-early Proterozoic time.     

Zircon SHRIMP U-Pb ages of the “Xinghuadukou Group” in Hanjiayuanzi and Xinlin areas and the “Zhalantun Group” in Inner Mongolia, Da Hinggan Mountains

A report is presented of SHRIMP zircon U-Pb dating data of meta-igneous and meta-sedimentary rocks of the Xinghuadukou Group(Xinlin-Hanjiayuanzi area,Heilongjiang Province)and meta-volcanic rocks of the Zhalantun Group(Zhalantun district,Inner Mongolia).The SHRIMP analyses show that the meta-igneous rocks from the Xinghuadukou Group formed at 506±10―547±46 Ma,belonging to Early-Middle Precambrian,whereas the meta-sedimentary rocks yielded detrital zircons,with ages of 1.0―1.2,1.6―1.8 and 2.5―2.6 Ga,indicative of deposition age at least<1.0 Ga. Meta-basic volcanic rocks from the Zhalantun Group have a formation age of 506±3 Ma.These data suggest that both the Xinghuadukou and Zhalantun Groups formed during Cambrian and/or Neoproterozoic time,rather than Paleoproterozoic time as previously thought.Early Precambrian inherited zircons in the meta-igneous rocks and numerous Precambrian detrital zircons in the meta-sedimentary rocks imply that these rocks were formed proximal to older crust.It is inferred that the Xinghuadukou and Zhalantun Groups represent Cambrian and/or Neoproterozoic vol- cano-sedimentary sequences formed in an active continental margin setting.     

Discovery of ∼4.0 Ga detrital zircons in the Aermantai ophiolitic mélange, East Junggar, northwest China

The East Junggar is an important part of the Central Asian Orogenic Belt(CAOB).Using in situ zircon dating and Hf isotopic analysis by LA-ICP-MS and MC-ICP-MS,respectively,a detrital zircon of 4040 Ma age was found in sedimentary sequences from the Aermantai ophiolitic mélange,East Junggar.This is the oldest age record in the East Junggar terrane,and also marks the first zircon locality in the CAOB with an age older than 4.0 Ga,which is attributed to the Hadean crust.The 4040 Ma detrital zircon has anεHf(t)value of–5.2 and a two-stage Hf modal age of 4474 Ma,suggesting the presence of very old(Hadean)crustal material in the source area.Beside peak ages of 446 Ma,we found four age groups of 3.6–3.1 Ga,2.53–2.37 Ga,1.14–0.89 Ga and 0.47–0.42 Ga from 141 effective measuring points.The age of 426±4 Ma for the five youngest detrital zircons defines the lower limit of the deposition time of sedimentary sequencess in the Aermantai ophiolitic mélange.The 0.47–0.42 Ga zircons exhibit176Hf/177Hf ratios of 0.282156 to 0.282850,corresponding to variableεHf(t)values from–9.3 to 12.0 and Hf model ages from2011 to 646 Ma.These characteristics are similar to those of the early Paleozoic igneous and gneissic zircons from the Altai,but significantly different from those of the East Junggar.Based on the material structures of felspathic greywacke,the morphology,internal texture and age distributions of dated detrital zircons,in combination with a study of the regional geological data,it is suggested that the sedimentary sequences in the Aermantai ophiolitic mélange was deposited in the Late Silurian,with the main provenance from the Altai Orogen in the north.This indicates that the early Paleozoic ocean represented by the Aermantai ophiolitic mélange was readily closed during the Late Silurian,and the northern edge of the East Junggar terrane was accreted to the Altai Orogen.The joint of them then served as a marginal orogen in the southern edge of the Siberia Paleocontinent.     

LA-ICP-MS U–Pb geochronology of detrital zircons from the Zhaochigou Formation-complex in the Helan Mountain and its tectonic significance

This paper carries out studies about LA-ICPMS U–Pb dating and Hf isotopic compositional analysis for detrital zircons in two metasedimentary samples that were taken from the Zhaochigou Formation-complex in the Helan Mountain.The results show that the Zhaochigou Formation-complex formed*1.96 Ga,and it is a part of the Khondalite Series that is widespread in the North China Craton(NCC).The age spectrum of the detrital zircons indicates that the Zhaochigou Formation-complex shared the same provenance with the eastern edge of the Khondalite Series.Products of ancient magmatic activities within the Khondalite Belt may be the major source for the sedimentary materials that formed the Khondalite Series.Our age-dating results suggest that the Khondalite Series in the NCC may have experienced two stages of metamorphism,as the early stage occurred during 1.96–1.95 Ga,and the later stage occurred at about 1.87 Ga.The Hfisotopic data indicate that the Western Block of the NCC endured a stage of crustal growth at 2.5–2.3 Ga.     

Zircon U-Pb SHRIMP dating for the volcanic rocks of the Xiong’er Group: Constraints on the initial formation age of the cover of the North China Craton

The volcanic rocks of the Xiong’er Group occurringwidely in the southern part of the North China Craton,overlay the Archean and Paleo-Proterozoic crystallinebasement and are overlain by middle to late Paleozoicterrigenous detrital rocks, carbonate and tillite. TheXiong’er Group crops out over an area of more than60000 km2 in a thickness ranging from 3000 to 7000 m,the largest magmatism after the formation of the crystal-line basement of the North China Craton (Fig. 1(a)). TheXiong’er …     

4.1 Ga old detrital zircon in western Tibet of China

4.1 Ga old detrital zircon was found by SHRIMP U-Pb dating for quartz schist from Buring County in western Tibet, Southwest China. This is the oldest zircon U-Pb age found in China so far. The detrital zircon is a zircon of magmatic origin because its Th/ U ratios are 0.76 to 0.86. Two dates older than 4.0 Ga were measured only in one grain. U-Pb ages of 35 measured spots in 24 zircons can be subdivided into 6 groups, corresponding to at least 6 episodes of magmatic activity in the target area. The present results provide an important geochronological constraint on the geological evolution of Qinghai-Tibet Plateau.     

Formation ages and source regions of the Palaeoproterozoic Gaofan,Hutuo and Dongjiao groups in the Wutai and Dongjiao areas of the North China Craton from SHRIMP U-Pb dating of detrital zircons: Resolution of debates over their stratigraphic relationships

This paper reports detrital zircon age distributions of meta-sedimentary rocks of the Gaofan, Hutuo and Dongjiao groups in the Wutai and Dongjiao areas of the North China Craton. Detrital zircons of a quartzite from the Gaofan Group are mainly ~2.5 Ga in age, with some ~2.7 Ga and older. A quartzite pebble from the basal conglomerate of the Hutuo Group is similar in detrital zircon age distribution to the quartzite of the Gaofan Group. For a meta-feldspar-quartz sandstone from the Dongjiao Group, the age of...     

Early Precambrian tectonothermal events of the North China Craton: Constraints from in situ detrital zircon U-Pb, Hf and O isotopic compositions in Tietonggou Formation

Clastic sediments and sedimentary rocks are widely used for understanding the formation and evolution of the continental crust. The Tietonggou Formation outcrops in the Xiaoqinling region at the southern margin of the North China Craton (NCC) and has unconformable contacts with the underlying Taihua Complex and overlying Paleoproterozoic Xiong’er Group. It mainly consists of quartzite and its protoliths are mature terrigenous clastic rocks. On the basis of the ages of the youngest detrital zircons from the quartzites and the ages of the Xiong’er Group, the depositional ages of the protoliths of the Tietonggou Formation were well constrained to 1.91–1.80 Ga. The U-Pb isotopic data of detrital zircons from the Formation show a major age peak at ～2.1 Ga, which is consistent with 2.2–2.0 Ga magmatism in the Trans-North China Orogen of the NCC. Taking into account the texctural and compositional maturity of the Tietonggou Formation quartzite, the ～2.1 Ga lithologic units in the Trans-North China Orogen are interpreted as the major source of the Tietonggou Formation. The majority of these ～2.1 Ga detrital zircons mostly have high δ ¹⁸O values (>6.5‰) and negative ? _Hf(t) values (?7.8–0.0), with corresponding Hf model ages significantly older than their crystallization ages, indicating that these zircons formed from the partial melting of ancient continental crust. The majority of the 2.8–2.7 Ga and ～2.5 Ga detrital zircons from the Tietonggou Formation had positive ? _Hf(t) values, and mantle-like δ ¹⁸O values, suggesting that the NCC has experienced two stages of significant crustal growth in the Neoarchaean at 2.7 and 2.5 Ga, respectively. The Hf isotopic data of detrital zircons from Paleoproterozoic metasedimentary rocks in the Trans-North China Orogen varied mainly toward the reduction of the radiogenic Hf isotope and gradually show a similar trend of the isotope trajectories of crustal evolution. This reveals that the NCC probably has not developed a long-lived subduction to complete the final assembly of the NCC. Alternatively, these maybe imply that the tectonic setting of the NCC substantially changed at ～2.1 Ga, the reduction of the radiogenic Hf isotope could be attributed to the rollback of the subducting slab.     

LA-(MC)-ICPMS U-Pb zircon geochronology and Lu-Hf isotope compositions of the Taihua complex on the southern margin of the North China Craton

Widely distributed on the southern margin of the North China Craton, the Taihua complex extends roughly in an east-west direction and the relatively complete successions are found in Lushan County, Henan Province. Like many other Archean terranes, the Taihua Complex can be divided into two major lithological units along the Dangze River, namely gneisses series and supracrustal rocks. The former is located on the north side of the river and chiefly composed of TTG gneisses and amphibolites; the latter on the south side of the river is mainly supracrustal rock. Coupled with the previous studies, the results obtained by this study show that the Taihua complex was formed in a large time span from Neoarchean to Palaeoproterozoic. The TTG gneisses and amphibolites are dated at Neoarchean (2794–2752 Ma). The 2.9 Ga and 3.1 Ga zircons in amphibolites could be xenocrysts. In the North China Craton, the 2.8–2.7 Ga old rocks crop out in several areas e.g. western Shandong Province, Jiaodong Peninsula and Lushan area of Henan Province. In addition, 2.8–2.7 Ga detrital zircons or xenocryst zircons have been recognized in Huai’an, Fuping, Wutai areas of North China Craton and also reported in the Early Paleozoic diamondiferous kimberlites in Mengyin and Fuxian. All these age results indicate that the 2.8–2.7 Ga rocks may have been developed much broader region than today’s outcrops. Zircon Hf and whole rock Nd isotopes show that the 2.8–2.7 Ga tectono-thermal event represents an important period of crustal growth with minor ancient crust reworked in the North China Craton. However the formation of supracrustal rocks is limited to 2.2–2.0 Ga in the Palaeoproterozoic time, not the Archaean, as previously believed. Combined with the chronological data of aluminium-rich metamorphic rocks (Khondalite series) on the southern margin of the North China Craton and adjacent areas, it is suggested that the above areas have widely developed Paleoproterozoic passive continental margin environment.     

Activation of northern margin of the North China Craton in Late Paleozoic: Evidence from U-Pb dating and Hf isotopes of detrital zircons from the Upper Carboniferous Taiyuan Formation in the Ningwu-Jingle basin

LA-MC-ICPMS U-Pb dating has been performed on detrital zircons from the Upper Carboniferous Tai-yuan Formation (N-8) in the Ningwu-Jingle Basin, west of the North China Craton (NCC). The ages of 72 detrital zircon grains are divided into three groups: 303―320 Ma (6 grains), 1631―2194 Ma (37 grains, peaked at 1850 Ma), 2318―2646 Ma (29 grains, peaked at 2500 Ma). Detrital zircons of Group 2 and Group 3 were likely derived from the basement of the NCC. Group 1 zircons exhibit 176Hf/177Hf ratios ranging from 0...     

U-Pb dating of detrital zircons from the Wudangshan Group in the South Qinling and its geological significance

U-Pb dating was made by the LA-ICP-MS method for detrital zircons from the Wudangshan volcanic-sedimentary succession in the South Qinling. Samples comprise quartz sandstones of the Wudangshan Group collected from the base of the Yangping Formation and an upper layer of the Shuangtai Formation overlain its volcanic sequence, and two river-sand collections from the drainage systems cutting across the two formations, respectively. The results show that the Yangping detrital zircons are dominated by 830–780 Ma grains with a minor population of ~1.0–0.84 Ga and sporadic grains of ~2.6, ~2.4 and 2.0 Ga, whereas the Shuangtai zircons yield an upper intercept age of 763±33 Ma, identical to the timing of the Wudangshan volcanism within error, with few concordant grains of 1.9 and 0.86 Ga. Age spectra for the two river-sand samples are similar to those of the Yangping and Shuangtai Formations, respectively. It thus suggests that the Wudangshan strata are less than 780 Ma, whereas their major detrital zircon populations of 1.0–0.85 Ga and 830–780 Ma are consistent with timing of the Hannan magmatic activities along the northwestern margin of the South China Block. This suggests a Hannan or adjacent area provenance for the Wudangshan strata. The Wudang area is characterized by rift-related igneous events at ~755 and ~680 Ma, respectively, pointing to a tectono- magmatic history different from the Hannan area. It is inferred that the ~755 Ma magmatism is likely to indicate a separation of the South China Block from the supercontinent Rodinia, while the ~680 Ma event suggests a further split between the South Qinling and some unknown continent.