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1.
本文通过低压MOCVD方法,采用改进的两步法工艺,即基片表面的高温处理一生长过渡层-退火-外延生长-退火工艺,在向[011]方向偏3°的Si(100)衬底上生长了GaAs膜,并对外延膜进行了X射线衍射,喇曼散射和光致发光分析.发现X射线衍射曲线光滑尖锐,无杂峰,(400)峰的摇摆曲线很锐,喇曼散射谱中TO峰与LO峰的强度比lTO/lLO很小,光致发光谱的半峰宽只有12.4meV,说明在Si上异质外延的GaAs单晶膜具有相当好的质量.  相似文献   

2.
采用溶胶-凝胶法,以较传统方法低的温度合成了Y2SiO5Ce3+纳米微晶,用X射线衍射、透射电子显微镜测定它们的物相为单斜晶系的Y2SiO5,平均粒径为30-40nm左右.还通过激发光谱和发射光谱,研究了其光致发光特性,观察到样品的发射谱的峰值波长位于458nm附近,比以固相反应法制备的Y2SiO5Ce3+微晶粉及单晶Y2SiO5Ce3+红移40nm左右.  相似文献   

3.
利用气相蒸发技术成功的制备了两个CuCl团簇薄膜样品.CuCl团簇被沉积到单晶Si和石英衬底上,然后覆盖一层NaCl以防氧化.通过透射电镜和选区衍射观察得知,两个样品主要由CuCl纳米晶和少量的Cu聚集体构成,其中CuCl纳米晶的直径分别约为3nm和6nm;通过室温下测得的光吸收和荧光光谱,发现CuCl激子吸收峰并未出现,而荧光峰向低能方向移动,这可能是激子声子强相互作用引起的结果.在77K温度观察到由激子声子耦合而展宽的荧光峰,其峰值近似与量子限制模型的计算结果一致,同时观察到来自陷阱态的宽峰.通过比较300K温度下激子荧光峰的展宽和红移量,发现团簇尺寸小的薄膜样品(3nm)中激子声子相互作用更强,这与理论预测定性一致  相似文献   

4.
采用常规X射线光电子能谱和同步辐射光电子能谱分别研究了超导系列样品Bi2Sr2Ca1-xPrxCu2O8+δ的芯能级谱和价带谱,讨论了这一系列样品电子结构变化的机制.实验发现随着Pr的掺杂,各芯能级谱和价带谱的位移都不同,根据Ca2p谱的变化规律,可认为Pr离子主要占据Ca离子格位  相似文献   

5.
C60Br24粉末单晶的制备及X—射线衍射分析   总被引:1,自引:1,他引:0  
介绍了制备C60Br24粉末单晶的新方法.用气相法制备出C60单晶颗粒.X-射线衍射分析表明制得的颗粒是纯C60单晶.然后用液体溴浸润C60单晶颗粒.72h后形成C60Br24单晶颗粒.样品在65℃下退火18h,以除去未反应的溴和使C60Br24分子排列规整.退火后样品的X-射线衍射谱较复杂,因为样品中还有无序的溴分子存在.于是将样品在相同退火温度下再退火36h.元素分析和红外光谱分析均表明经54h退火后的样品成分是C60Br24,它的X-射线衍射谱显然要清晰得多.对该衍射谱的最佳拟合得出C60Br24单晶为正交面心结构,其晶格常数为a=2.156nm,b=1.675nm,c=1.294nm.  相似文献   

6.
利用MEVVA离子源进行离子束合成,制备了C^+离子注入单晶Si衬底的样品,并利用椭偏光谱法研究了退火和未退火两种情况。椭偏光谱测量波长范围为400 ̄2000nm。通过对所测量样品的椭偏光谱数据分析,可得到离子束合成SiC/Si异质结构的多层膜结构。椭偏光谱法的测量结果证实:退火样品形成了SiC埋层,即使进行高温、长时间退火处理,该埋层SiC仍难以得到SiC体材料的光学常数。  相似文献   

7.
研究和建立了CPA矩阵-分光光度法同时测定动植物细胞赋活剂(丰产素)中的四种有机组分的新方法,确定了实验条件,选择450,410,400,380,360,340,320及300nm8个波长为矩阵波长列,方法简便、快速、准确,样品测定中对各组分的相对偏差在0.48%~3.80%范围;回收率在99%~105%范围。  相似文献   

8.
研究和建立了CPA矩阵-分光光度法同时测定动植物细胞赋活剂中的四种有机组分的新方法,确定了实验条件,选择450,410,400,380,360,340,320及300nm8个波长为矩阵波长列,方法简便,快速、准确,样品测定中对各组分的相对偏差在0.48%-3.80%范围,回收率在99%-105%范围。  相似文献   

9.
采用分子束外延(MBE)方法生长了GexSi1-x/Si应变超晶格.利用X射线双晶衍射、小角衍射和宽角衍射方法测量了超晶格样品的实验衍射曲线.运用X射线运动学理论和动力学理论,分析、模拟了样品的实验曲线,得到了精确的定量结构参数数据.并根据实验曲线中衍射峰的位置和分布情况对应变超晶格的生长质量做了评价.  相似文献   

10.
高温热解聚硅烷制备SiC薄膜初探   总被引:1,自引:0,他引:1  
用组合成的可溶性聚硅烷1710A作涂膜材料,进行不同温度的真空热解或高纯氮下热解实验。通过IR谱和XPS谱分析,在790-810cm^-1和1270cm^-1红外吸收特征峰分别对应Si-CH3摇摆振动和伸缩振动吸收峰,XP-Si谱给出Si(2P)结合能力为101.6eV,CIS为284.3eV,证明有α-SiC:H生成。  相似文献   

11.
There are numerous geometric objects stored in the spatial databases. An importance function in a spatial database is that users can browse the geometric objects as a map efficiently. Thus the spatial database should display the geometric objects users concern about swiftly onto the display window. This process includes two operations:retrieve data from database and then draw them onto screen. Accordingly, to improve the efficiency, we should try to reduce time of both retrieving object and displaying them. The former can be achieved with the aid of spatial index such as R-tree, the latter require to simplify the objects. Simplification means that objects are shown with sufficient but not with unnecessary detail which depend on the scale of browse. So the major problem is how to retrieve data at different detail level efficiently. This paper introduces the implementation of a multi-scale index in the spatial database SISP (Spatial Information Shared Platform) which is generalized from R-tree. The difference between the generalization and the R-tree lies on two facets: One is that every node and geometric object in the generalization is assigned with a importance value which denote the importance of them, and every vertex in the objects are assigned with a importance value,too. The importance value can be use to decide which data should be retrieve from disk in a query. The other difference is that geometric objects in the generalization are divided into one or more sub-blocks, and vertexes are total ordered by their importance value. With the help of the generalized R-tree, one can easily retrieve data at different detail levels.Some experiments are performed on real-life data to evaluate the performance of solutions that separately use normal spatial index and multi-scale spatial index. The results show that the solution using multi-scale index in SISP is satisfying.  相似文献   

12.
13.
Future mobile communication systems aim at providing very high data transmission rates, even in high-mobility scenarios such as high-speed wheel-track trains, maglev trains, highway vehicles, airplanes, guided missiles or spacecraft. A particularly important commercial application is the strong and increasing worldwide demand for high- speed broadband wireless communications (up to 574.8 km/ h test speeds or 380 km/h commercial speeds) in railways, providing data, voice and video services for applications such as onboard entertainment services to passengers, train control, train dispatch, train sensor status handling and sur- veillance. In such high-mobility scenarios, there are a number of communication challenges, including fast hand- over, location updating, high-speed channel modeling, estimation and equalization, anti-Doppler spreading tech- niques, fast power control, and dedicated network architec- ture. Because signal transmission in very high-speed scenarios will inevitably experience serious deterioration, it is imperative to develop key broadband mobile communi- cation techniques for such high-speed vehicles.  相似文献   

14.
Instead of following Fock’s expansion,we solve the Schrodinger equation for some quantum mechanical manybody systems such as electrons in atoms and charged excitons in quantum wells in a similar way in hyperspherical coordinates by expanding the wave functions into orthonormal complete basis sets of the hyperspherical hannonics(HHs)of hyperangles and generalized Laguerre polynomials(GLPs)of the hyperradius.This leads the equation to  相似文献   

15.
Being the primary media of geographical information and the elementary objects manipulated, almost all of maps adopt the layer-based model to represent geographic information in the existent GIS. However, it is difficult to extend the map represented in layer-based model. Furthermore, in Web-Based GIS, It is slow to transmit the spatial data for map viewing. In this paper, for solving the questions above, we have proposed a new method for representing the spatial data. That is scale-based model. In this model we represent maps in three levels: scale-view, block, and spatial object, and organize the maps in a set of map layers, named Scale-View, which associates some given scales.Lastly, a prototype Web-Based GIS using the proposed spatial data representation is described briefly.  相似文献   

16.
为了有助于提高英文爱好者的个人情操、文化素养和学习兴趣,以及专业人员对英语学习和研究进行多途径的探索,本文通过一些精选诗歌的引证和分析,着重论述了喻类修辞法在英文诗歌中的运用其及效果。  相似文献   

17.
Tennessee Williams is considered as one of the most important American playwrights since World War II.The Glass Menagerie is his first successful drama,which describes a tragic situation of family and means to say that Man is unable to change the miserable life,no matter whatever means he try,This essay focuses on the analysis of the arrangement of the four main characters:Laura.Amanda,Jim and Tom to reveal the theme.Laura is fragile.Amanda is brave.Jim is vital.Tom is sensible.And all of them develop and try the different means to struggle against life,but fail tragically.With the evidence,the paper comes to conclusion naturally that Man is unable to change the miserable life,and he dooms to fail.  相似文献   

18.
The aim of this study is to investigate the diversity of Retama raetam root-nodule bacteria isolated from arid regions of Tunisia. Twelve isolates, chosen as representative for different 16S rRNA gene patterns, were characterized by 16S rRNA gene sequencing and phenotypic analysis. Isolates were assigned to Sinorhizobium, Rhizobium and Agrobacterium. Symbiotic properties of Sinorhizobium and Rhizobium isolates showed a large diversity in their capacity to infect their host plant and fix atmospheric nitrogen. Strain RK 22 identified as Rhizobium was the most effective isolate.  相似文献   

19.
正Recently,docking has been widely used to predict the binding-modes of protein-inhibitors,when the crystal complexes structure was absent.Most docking algorithms are able to generate a large number of probable conformations,it,however,is difficult to effectively evaluate these docking poses and identify the most reasonable bindingmode.In the present study,on the basis of the crystallographic data of human 3-hydroxy-3-methylglutaryl coenzyme  相似文献   

20.
介绍了WiMAX与Wi-Fi两种无线宽带接入技术,并对两者之间的关系及相互之间的影响做了对比及分析,并对WiMAX的关键技术进行了详细说明,最后对两者的联合组网方式做了简单的探讨。  相似文献   

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