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1.
采用化学共沉淀法制备了掺钕钛酸铋陶瓷粉料,对其相组成和形貌进行研究,进而制备块体陶瓷,对其电学性能和疲劳特性进行分析.结果表明:粉料经550℃烧结后开始结晶,随烧结温度的进一步提高,结晶逐步完善而形成单相层状钙钛矿结构.块体材料的2Pr和Ec值分别为12.56μC/cm2和29.9 V/cm.经过1011次读/写循环后BNT的Pr值基本上没有下降,说明材料具有良好的抗疲劳特性.  相似文献   

2.
采用溶胶凝胶法在一定条件下合成组成为0.91SrTiO_3+0.09(Bi_2O_3·3TiO_2)的高纯、超细陶瓷粉料。该粉料添加PbO.Li_2O,Cs_2O等物质.可制成高质量改性SrTiO_3电容器材料。用此法制备的电容器材料可大大地降低合成温度,经改性后可使其烧结温度展宽,并具有较为理想的介电常数和介电损牦。  相似文献   

3.
采用溶胶-凝胶法制备了La2/3Sr1/3MnO3多晶样品.X射线衍射测试结果表明样品具有钙钛矿结构.利用振动样品磁强计测量了粉体样品在室温下的磁性能,样品表现为铁磁性.对不同烧结温度下形成的块体样品的导电性以及磁电阻的研究表明,随着烧结温度的提高材料的金属-绝缘体转变温度有所增加,说明材料的烧结温度对其电导性有很大的影响.  相似文献   

4.
用表面包覆8wt%TiO2纳米粉末的微米Al90Mn9Ce1合金复合粉末,制备了高致密的闭合微胞陶瓷结构,内充金属合金的块体复合材料,烧结温度仅为520℃,烧结后的致密度达到98.2%。SEM观察结果显示,该材料的陶瓷胞壁厚度约为1.0~2.0μm,胞体尺寸约为15~40μm,经10%HCl深腐蚀后,留下完整的微胞状陶瓷骨架。根据实验结果,对SPS烧结微-纳米混合粉体的瞬时界面烧结机理进行探讨。  相似文献   

5.
研究了用Sol-Gel法制备粉料和气氛烧结KTN陶瓷的优化工艺.通过分析烧结气氛和烧结条件对KTN陶瓷性能的影响,指出相应的最佳烧结温度为1200℃、保温时间为87h.  相似文献   

6.
应用传统的陶瓷制备工艺制备Ba0.7Sr0.3TiO3陶瓷靶材,讨论了Ba0.7Sr0.3TiO3陶瓷靶材的最佳工艺条件.用XRD衍射仪分析了预烧粉料的物相结构,并结合热失重(TG)分析确定了BST(70/30)粉料的预烧温度,用SEM观察了Ba0.7Sr0.3TiO3陶瓷靶材在不同烧结温度下的显微结构,用Agilent 4294A精密阻抗分析仪测得BST靶材的介电性能,用Precise-Workshop测试BST靶材的铁电性能.实验结果表明,采用传统的陶瓷制备工艺制得晶粒较为均匀、结构致密的Ba0.7Sr0.3TiO3陶瓷靶材的最佳工艺条件为:在940℃预烧2h,13000C烧结2h.  相似文献   

7.
机械合金化制备Ti2SnC粉体,采用放电等离子烧结(SPS)技术制备致密的Ti2SnC块体。研究烧结温度对机械活化SPS烧结Ti2SnC导电陶瓷块体致密化影响。结果表明,机械合金化合成Ti2SnC粉体经烧结后,气孔率随温度的升高逐渐降低。在900-1000℃之间进行SPS烧结可以获得纯度较高的块体。当温度在600-900℃范围内时,密度随烧结温度的提高而逐渐增大,当温度进一步提高时,则略呈下降趋势。  相似文献   

8.
HAP生物活性陶瓷的结构稳定性与力学性能   总被引:1,自引:0,他引:1  
探讨了羟基磷灰石生物活性陶瓷的制备工艺对材料结构稳定性及力学性能的影响。采用化学共沉淀法合成羟基磷灰石粉料,采用注浆成型、热压烧结及热等级压后烧结等工艺制备羟基磷灰石颌面骨材料。经结构分析、力学性能测试及显微结构观察,认为该材料具有满足于临床应用的物理性能。  相似文献   

9.
以TiO_2、Fe_2O_3和Bi_2O_3为原料,采用固相反应法分别在975、1 000、1 025、1 050℃下烧结制备Bi_5Ti_3FeO_(15)(BTFO)多铁陶瓷.X线衍射结果显示,不同烧结温度制备的BFTO陶瓷均为单一的层状钙钛矿相.随着烧结温度的升高,BTFO陶瓷的晶粒尺寸增大,致密度提高.扫描电镜的结果表明1 050℃烧结的陶瓷样品,晶粒尺寸约为15μm,具有最大的剩余极化Pr值18.6μC/cm~2.BTFO陶瓷在室温下为顺磁性,同时具有一定的磁电耦合特性,磁场为725 Oe、频率50Hz下测得的磁电耦合系数达到3.7 m V/cm Oe.  相似文献   

10.
在刚玉粉料中添加纳米二氧化硅,利用原位合成方法制备了氧化铝基复合陶瓷型芯,讨论了纳米二氧化硅含量以及烧结制度对氧化铝基复合陶瓷型芯烧结温度、室温强度、高温蠕变等性能的影响.结果表明:SiO2纳米粉的加入,使陶芯材料致密度增加,从而使陶芯烧结温度降低,陶芯室温强度大幅度提高;随着SiO2含量加大,线收缩率和相对密度增加,...  相似文献   

11.
There are numerous geometric objects stored in the spatial databases. An importance function in a spatial database is that users can browse the geometric objects as a map efficiently. Thus the spatial database should display the geometric objects users concern about swiftly onto the display window. This process includes two operations:retrieve data from database and then draw them onto screen. Accordingly, to improve the efficiency, we should try to reduce time of both retrieving object and displaying them. The former can be achieved with the aid of spatial index such as R-tree, the latter require to simplify the objects. Simplification means that objects are shown with sufficient but not with unnecessary detail which depend on the scale of browse. So the major problem is how to retrieve data at different detail level efficiently. This paper introduces the implementation of a multi-scale index in the spatial database SISP (Spatial Information Shared Platform) which is generalized from R-tree. The difference between the generalization and the R-tree lies on two facets: One is that every node and geometric object in the generalization is assigned with a importance value which denote the importance of them, and every vertex in the objects are assigned with a importance value,too. The importance value can be use to decide which data should be retrieve from disk in a query. The other difference is that geometric objects in the generalization are divided into one or more sub-blocks, and vertexes are total ordered by their importance value. With the help of the generalized R-tree, one can easily retrieve data at different detail levels.Some experiments are performed on real-life data to evaluate the performance of solutions that separately use normal spatial index and multi-scale spatial index. The results show that the solution using multi-scale index in SISP is satisfying.  相似文献   

12.
Language markedness is a common phenomenon in languages, and is reflected from hearing, vision and sense, i.e. the variation in the three aspects such as phonology, morphology and semantics. This paper focuses on the interpretation of markedness in language use following the three perspectives, i.e. pragmatic interpretation, psychological interpretation and cognitive interpretation, with an aim to define the function of markedness.  相似文献   

13.
14.
Future mobile communication systems aim at providing very high data transmission rates, even in high-mobility scenarios such as high-speed wheel-track trains, maglev trains, highway vehicles, airplanes, guided missiles or spacecraft. A particularly important commercial application is the strong and increasing worldwide demand for high- speed broadband wireless communications (up to 574.8 km/ h test speeds or 380 km/h commercial speeds) in railways, providing data, voice and video services for applications such as onboard entertainment services to passengers, train control, train dispatch, train sensor status handling and sur- veillance. In such high-mobility scenarios, there are a number of communication challenges, including fast hand- over, location updating, high-speed channel modeling, estimation and equalization, anti-Doppler spreading tech- niques, fast power control, and dedicated network architec- ture. Because signal transmission in very high-speed scenarios will inevitably experience serious deterioration, it is imperative to develop key broadband mobile communi- cation techniques for such high-speed vehicles.  相似文献   

15.
Instead of following Fock’s expansion,we solve the Schrodinger equation for some quantum mechanical manybody systems such as electrons in atoms and charged excitons in quantum wells in a similar way in hyperspherical coordinates by expanding the wave functions into orthonormal complete basis sets of the hyperspherical hannonics(HHs)of hyperangles and generalized Laguerre polynomials(GLPs)of the hyperradius.This leads the equation to  相似文献   

16.
Being the primary media of geographical information and the elementary objects manipulated, almost all of maps adopt the layer-based model to represent geographic information in the existent GIS. However, it is difficult to extend the map represented in layer-based model. Furthermore, in Web-Based GIS, It is slow to transmit the spatial data for map viewing. In this paper, for solving the questions above, we have proposed a new method for representing the spatial data. That is scale-based model. In this model we represent maps in three levels: scale-view, block, and spatial object, and organize the maps in a set of map layers, named Scale-View, which associates some given scales.Lastly, a prototype Web-Based GIS using the proposed spatial data representation is described briefly.  相似文献   

17.
为了有助于提高英文爱好者的个人情操、文化素养和学习兴趣,以及专业人员对英语学习和研究进行多途径的探索,本文通过一些精选诗歌的引证和分析,着重论述了喻类修辞法在英文诗歌中的运用其及效果。  相似文献   

18.
Tennessee Williams is considered as one of the most important American playwrights since World War II.The Glass Menagerie is his first successful drama,which describes a tragic situation of family and means to say that Man is unable to change the miserable life,no matter whatever means he try,This essay focuses on the analysis of the arrangement of the four main characters:Laura.Amanda,Jim and Tom to reveal the theme.Laura is fragile.Amanda is brave.Jim is vital.Tom is sensible.And all of them develop and try the different means to struggle against life,but fail tragically.With the evidence,the paper comes to conclusion naturally that Man is unable to change the miserable life,and he dooms to fail.  相似文献   

19.
The aim of this study is to investigate the diversity of Retama raetam root-nodule bacteria isolated from arid regions of Tunisia. Twelve isolates, chosen as representative for different 16S rRNA gene patterns, were characterized by 16S rRNA gene sequencing and phenotypic analysis. Isolates were assigned to Sinorhizobium, Rhizobium and Agrobacterium. Symbiotic properties of Sinorhizobium and Rhizobium isolates showed a large diversity in their capacity to infect their host plant and fix atmospheric nitrogen. Strain RK 22 identified as Rhizobium was the most effective isolate.  相似文献   

20.
理论推导与室内实验相结合,建立了低渗透非均质砂岩油藏启动压力梯度确定方法。首先借助油藏流场与电场相似的原理,推导了非均质砂岩油藏启动压力梯度计算公式。其次基于稳定流实验方法,建立了非均质砂岩油藏启动压力梯度测试方法。结果表明:低渗透非均质砂岩油藏的启动压力梯度确定遵循两个等效原则。平面非均质油藏的启动压力梯度等于各级渗透率段的启动压力梯度关于长度的加权平均;纵向非均质油藏的启动压力梯度等于各渗透率层的启动压力梯度关于渗透率与渗流面积乘积的加权平均。研究成果可用于有效指导低渗透非均质砂岩油藏的合理井距确定,促进该类油藏的高效开发。  相似文献   

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