Impact chaos control and stress release? -A key for development of ultra fine vibration milling

Through our previous experimental and analytical studies, it has been discovered that the key for the development of vibration milling is the impact chaos control and stress release. The necessities for the chaos control and stress release are: (i) to strictly eliminate the sub-harmonics; (ii) to control the super-harmonics to a lower level and (iii) to load the system compressively with relatively higher period, in order that the vibration energy can be absorbed by the particles effectively and sufficiently. A new vibration model for ultra fine milling is proposed, which has wide applications in preparing ultra fine particles.     

Improved ethanol, acetone and H2 sensing performances of micro-sensors based on loose ZnO nanofibers

Both one-dimensional nanostructures and porous nanostructures are benefit to the sensing enhancement of semiconducting functional materials.The present paper shows an effective route to combining the advantages of these two nanostructures for a novel type of ZnO nanomaterials.Basically,a pore-forming material is employed in an electrospinning method,and the products are characterized by X-ray powder diffraction(XRD),energy dispersive X-ray spectroscopy(EDX),and transmission electron microscopy(TEM).The obtained materials are loose ZnO nanofibers,which own both porous and one-dimensional nanostructures.Micro-sensors are fabricated by sputtering and etching techniques,and the as-prepared nanofibers are used as the functional materials in them.The sensors show improved sensing properties both in sensitivity and response-speeds.The sensitivity is enhanced from 4 to 8 and the response time is shortened from 14 to 10 s when the sensors are exposed to 100 μL/L ethanol at 260℃.Similar results are also observed in acetone and H2 sensing tests.These enhancements are based on the one-dimensional and porous nanostructures of the nanofibers.     

Synthesis, characterization and antibacterial activity of copper, nickel and bimetallic Cu– Ni nanoparticles for potential use in dental materials

The antibacterial effect is a desirable property in dental materials.Development of simple methods for the preparation of nanosized metal particles has attracted significant attention because of their future applications due to unusual size-dependent antibacterial properties.Copper(Cu),Nickel(Ni) and bimetallic Cu–Ni nanoparticles were prepared by a simple chemical method and their antibacterial activity was tested against the widely used standard human pathogens Staphylococcus aureus(gram-negative) and Escherichia coli(gram-positive).Additionally,these nanoparticles were tested against the dental pathogen Streptococcus mutans.Our results are promising for potential use in dental materials science.     

Nonlinear Transversal Vibration Analysis of an Axially Moving Viscoelastic Yarn in Tufting Process

The nonlinear transversal vibration of axially moving yarn with time-dependent tension is investigated. Yarn material is modeled as Kelvin model. A partial differential equation governing the transversal vibration is derived from the Newton＇s second law. Galerkin method is used to truncate the governing nonlinear differential equation, and thus the first.order ordinary differential equation is obtained. The periodic vibration equation and the natural frequency of moving yarn are received by applying homotopy perturbation method. As a result, the condition which should be avoided during the tufting process for resonance is obtained.     

A new way of transformation from α-quartz to coesite

A laboratory method combining the high-energy mechanical ball milling and high static pressure has been suggested for modelling synthesis of coesite in the Earth’s crust. A window of milling time, a mechanical collision-induced intermediate phase of α-quartz and its condition of easily crystallizing into coesite under the condition of 3.0 GPa, 923 K, < 1.0 min have been discovered. The new method needs much shorter synthesizing time and lower synthesizing critical pressure than those used before. The Raman spectra for the coesite synthesized by the present method have covered all the information of those natural and synthesized coesites reported before. It is demonstrated that this method has a great potential in geo-science research and implied the other possible mechanism of coesite formation in the Earth’s crust.     

A new way of transformation from α-quartz to coesite

A laboratory method combining the high-energy mechanical ball milling and high static pressure has been suggested for modelling synthesis of coesite in the Earth’s crust. A window of milling time, a mechanical collision-induced intermediate phase of α-quartz and its condition of easily crystallizing into coesite under the condition of 3.0 GPa, 923 K, < 1.0 min have been discovered. The new method needs much shorter synthesizing time and lower synthesizing critical pressure than those used before. The Raman spectra for the coesite synthesized by the present method have covered all the information of those natural and synthesized coesites reported before. It is demonstrated that this method has a great potential in geo-science research and implied the other possible mechanism of coesite formation in the Earth’s crust.     

数控机床切削振动的动态性能试验分析

以一数控弧齿锥齿轮铣齿机为例，研究机床结构振动模态薄弱环节的确认方法，为结构改进提供依据、通过动态试验，测量机床刀具和工件间相对激振的频率响应曲线G（ω），并分析出机床结构存在两个薄弱模态振型．切削颤振试验表明，机床在切齿期间，系统结构存在不同的颤振频率，恰好和机床G（ω）的薄弱模态频率相对应．机床结构有限元模态和试验模态分析均验证了该结构薄弱模态的存在．     

中厚板轧机非线性参激的振动

建立了中厚板轧机两自由度非线性参激振动模型,分析了轧机振动系统在主参数共振情形下的振动特性,尤其是振动系统随激励参数变化的拟周期振动和混沌运动现象。分析结果表明:轧制过程中轧制力的周期性变化可以导致轧机振动系统混沌运动的产生;避免激振力频率与系统固有频率相近,以防止混沌的出现。     

球磨对水热法制备锰锌铁氧体纳米粉体工艺的影响

以硝酸铁、硝酸锰、硝酸锌为原料,采用传统水热法和球磨辅助水热法合成了锰锌铁氧体纳米粉体,通过xRD、TG-DSC和TEM研究了粉体的结晶性能、热性能以及粉体的形貌,分析了机械球磨的加入对纳米粉体制备的影响。研究表明,球磨的加入可以明显提高晶化反应速度,在相同时间内制得的纳米晶发育好于传统水热法制得的锰锌铁氧体纳米晶。球磨对粉体的热性能影响很小。传统水热法和球磨辅助水热法均可制得粒径10nm左右的锰锌铁氧体纳米晶,但粉体的分散性球磨辅助水热法优于传统水热法。     

振动磨连续粉磨工艺

对物料在筒体内滞留时间和数量进行了试验研究，同时探讨了工作条件对产品粒度和处理量的影响．     

平面端铣切削振动实验观察与计算机仿真

在切削试验和计算机仿真中观察分析铣削强迫振动与自激振动现象，通过比较试验，仿真以及前人研究结果，表明数字仿真可行，有优越性，分析了振动影响因素仿真确定稳定性极限产生误差的原因，发现机床模太参数影响远大于切削力特征值，证明建立多质量多自由度等效系统模型的必要。探讨了铣削振动消减措施。     

立铣加工切削力和振动的计算机仿真与实验

在改进的非线性立铣加工铣削力数学模型和动力学方程基础上,采用变步长数值积分算法(四阶显式Runge-Kutta算法),建立动态铣削加工过程的计算机仿真模型.通过铣削加工动力学实验,对仿真模型输出的铣削力和铣削振动的时域特性预测精度进行验证,进一步对其频域特性进行分析.结果表明,该仿真模型作为高效低耗的研究平台,可较好地用于立铣加工铣削力与铣削振动的预估及其频域特性分析.     

干法室温振动制备超微颗粒的理论与应用

采用振动研磨的方法制备超微颗粒的理论研究表明,外力所作的功克服了材料的内聚力使材料发生局部变形,当局部应力超过临界剪切应力时产生断裂口,裂口的形成释放了物料内部的变形能,促使裂纹继续扩展形成新的表面,碰撞过程中振动能量转化为新生颗粒的表面能、热能和化学能.扫描电子显微镜和透射电子显微镜图像显示,研磨过程中固体颗粒于结构薄弱处发生塑性变形直至颗粒破碎,随着研磨时间的增加,颗粒不断细化,粒度分布趋于均匀.X射线衍射分析可见,样品的晶体结构和化学成分均未改变,颗粒细化过程中没有新物相产生.     

Impact chaos control and stress release -A key for development of ultra fine vibration milling

Through our previous experimental and analytical studies, it has been discovered that the key for the development of vibration milling is the impact chaos control and stress release. The necessities for the chaos control and stress release are: (i) to strictly eliminate the sub-harmonics; (ii) to control the super-harmonics to a lower level and (iii) to load the system compressively with relatively higher period, in order that the vibration energy can be absorbed by the particles effectively and sufficiently. A new vibration model for ultra fine milling is proposed, which has wide applications in preparing ultra fine particles.